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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell corn E-mail main @mccampbel I corn <br /> IAdvanced GeoEnvironmental Client Project ID Cherokee Truck Stop Date Sampled 03/20/00 <br /> 4005 North Wilson Way Date Received 03/23/00 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 03/25-03/28/00 <br /> Client P O Date Analyzed 03125-03/28/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 33736 <br /> Client 1D UST413-20-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone i NDt2 0 trans-l,3-Dichloropropene NO <br /> Benzene i NO Ethylene dibromide NO <br /> Bromobenzene NO Ethylbenzene NO <br /> Bromochloromethane NO Hexachlorobutadiene NO <br /> Bromodichloromethane NO lodomethane ND <br /> Bromoform NO Isopropylbenzene NO <br /> Bromomethane ND p Isopropyl toluene ND <br /> n-Butyl benzene NO Methyl butyl ketone NO <br /> sec-Butyl benzene NO Methylene Chloride" NDt2 0 <br /> tert-Butyl benzene NO Methyl ethyl ketone NO <br /> Carbon Disulfide NO Methyl isobutyl ketone ie NO <br /> Carbon Tetrachloride NO Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene NO Naphthalene NO <br /> Chloroethane NO n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" NO Styrene` ND <br /> Chloroform NO 1,1,1,2-Tetrachloroethane NO <br />' Chloromethane ND 1,1,2,2-Tetrachloroethane NO <br /> 2-hilorotoluene NO Tetrachloroethene NO <br /> 4-Chlorotoluene NO To—]uc n e"I NO <br />' Dibromochloromethane ND 1,2 3-Tnchlorobenzene NO <br /> 1,2-Dibromo-3-chioropropane NO 1,2,4-Trichlorobenzene NO <br /> Dibromomethane NO 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene NO 1,1,2-Trichloroethane NO <br />' 1,3-Dichlorobenzene ND Trichloroethene NO <br /> 1,4-Dichlorobenzene NO Tnchlorol)uoromethane NO <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane NO <br /> I,1-Dichloroethane NO 1,2,4-Tnmethylbenzene NO <br />' 1,2-Dichloroethane NO 1,3,5-Tnmethylbenzene NO <br /> 1,1-Dichloroethene NO Vinyl Acetate'° NO <br /> cis-1,2-Dichloroethene NO Vinyl Chloride"I ND <br /> trans 12-Dichloroethene NO Xylenes,totalNO <br />' 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane NO Surrogate Reco%cries(`%) <br /> 2 2-Dichloropropane NO Dibromofluoromethane 103 <br /> 1,1-Dichloropropene NO Toluene-d8 104 <br />' cis-1,3-Dichloropropene ND 4-Brornofluorobenzene 121 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated N ater samples I ug/L,vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg,m ipes 0 Zug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-prop2none or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane, (f) 2-butatione, (g) 4-methyl 2- <br /> pentanone or isoprop)Iacetone (h) lighter than water immiscible sheen is present, (i)hquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />