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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbellcam E-mail main@mccampbcll corn <br /> Advanced GeoEnvironmental Client Project ID Cherokee Truck Stop Date Sampled 03/20/00 <br /> 4005 North Wilson Way Date Received 03/23/00 <br /> IStockton,CA 95205 Client Contact Kevin McKibben Date Extracted 03/25-03/28/00 <br /> Client P O Date Analyzed 03/25-03/28/00 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 33737 <br /> Client ID UST5/3-20-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone t ND<40 trans-l,3-Dichloropropene ND<5 0 <br /> Benzene 17 Ethylene dibromide ND<5 0 <br /> Bromobenzene ND<5 0 Ethylbenzene N0<5 0 <br /> Bromochloromethane ND<5 0 1-lexachlorobutadtene ND<5 0 <br />' Bromodichloromethane ND<5 0 lodomethane ND<5 0 <br /> Bromofenn ND<5 0 Isopropylbenzene ND<5 0 <br /> Bromomethane ND<5 0 p4sopropyl toluene ND<5 0 <br /> n-Butyl benzene ND<5 0 Methyl butyl ketone ND<5 0 <br />' sec-Butyl benzene ND<5 0 Methylene Chlonde` ND<25 <br /> tert-Butyl benzene ND<5 0 Methyl ethyl ketone NDX5 0 <br /> Carbon Disulfide ND<5 0 Methyl isobutyl ketone`s ND<5 0 <br /> Carbon Tetrachlonde ND<5 0 Methyl ten-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<5 0 Naphthalene ND<5 0 <br /> Chloroethane ND<5 0 n-Propyl benzene ND<5 0 <br /> 2-Chloroethyl Vinyl Ether" ND<5 0 Styrene WND<5 0 <br /> Chloroform ND<5 0 1,1,1,2-Tetrachloroethane ND<5 0 <br />' Chloromethane ND<5 0 1,1,2,2-Tetrachl0roethane ND<5 0 <br /> 2-Chlorotoluene ND<5 0 Tetrachloroethane 14 <br /> 4-Chlorotoluene ND<5 0 Toluene ND<5 0 <br />' Dibromochloromethane ND<5 0 1,2,3-Tnchlorobenzene ND<5 0 <br /> 1,2-Dibromo-3-chloropropane ND<5 0 1,2,4-Tnchi orobenzene ND<5 0 <br /> Dibromomethane ND<5 0 1 ],I-Trichloroethane ND<5 0 <br /> 1 2-Dichlorobenzene ND<5 0 1 1,2-Trichloroethane ND<5 0 <br />' 1,3-Dichlorobenzene ND<5 0 Tnchloroethene ND<5 0 <br /> 1,4-Dichlorobenzene ND<5 0 Trichlorofluoromethane ND<5 0 <br /> Dichlorodifluoromethane ND<5 0 1,2,3 Trichloropropane ND<5 0 <br /> 1,1-Diehl oroethane ND<5 0 1,2,4-Trimethylbenzene ND<5 0 <br /> 1,2-Dichloroethane 160 1,3,5-Tnmethylbenzene NIX5 0 <br /> 1,l-Dichloroethene ND<5 0 Vinyl Acetate ') ND<5 0 <br /> cis-1,2-Dichloroethene ND<5 0 Vinyl Chloride " ND<5 0 <br /> trans-1,2-Dichloroethene ND<5 0 Xylenes,total ND<5 0 <br />' 1,2-Dtchloropropane NlX5 0 Comments <br /> 1,3-Dtchloropropane ND<5 0 Surrogate Reco i eves(%) <br /> 2,2-Dtchloropropane ND<5 0 Dibromofluoromethane 105 <br /> 1,1-Dichloropropene ND<50 Toluene-d8 103 <br />' cis-1,3-Dichloropropene ND<5 0 4-Bromofluorobenzcne 91 <br /> eater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> /reporting limits unless otherwise stated .Nater samples I ug/l, vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 Zug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g)4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />