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! Stockkon 99 Speedway <br /> Quality Assurance Project Plan April 12,2007 <br /> The laboratory selected for this work is certified to perform the requested analyses. The laboratory will <br /> i strictly adhere to state and federal requirements of the methods requested. <br /> The analytical methodologies, required equipment, laboratory procedures shall meet the standards for . <br /> the associated EPA' methodology. A summary of EPA methodologies and sample holding times is <br /> provided in Table 1. <br /> I <br /> 5.3 Quality Control <br /> QC procedures will be carried out during field sampling and laboratory analysis activities. QC procedures <br /> in the field will consist of strict protocols for field sampling and decontamination procedures (described in <br /> the PEA Workplan) and the collection of field blanks and blind split samples for laboratory analysis. <br /> Laboratory QC procedures will include the analysis of matrix spike and matrix spike duplicates. A <br /> description of the QC procedures is presented in the following sections. <br /> 5.3.1 Field QC Samples <br /> QC samples ensure that the sampling and field measurements activities are in control and generate <br /> quality data. QC samples for this project will consist of trip blanks, equipment blanks and duplicates/split. ' <br /> samples. <br /> • One trip blank will be collected per shipping container of samples during the course of the PEA. . <br /> The trip blank will be submitted to the laboratory for VOC analysis. The trip blank will consist of a <br /> sample vial that is filled in the laboratory with ASTM Type II reagent grade water, transported to <br /> the site, handled like a sample and returned to the laboratory for analysis. <br /> • Equipment blanks will be collected at a frequency of one per day per matrix, or a minimum of five <br /> percent of the samples collected. An equipment blank will be colleted by pouring ASTM Type II <br /> reagent grade water through or over the purging or sampling device, transferring the water to a <br /> sample bottle, and transporting it to the laboratory for analysis. <br /> • Field duplicates/splits will be collected for every 20 samples collected of each matrix. Field <br /> duplicates will be collected from one sampling location during a single act of sampling. The <br /> precision goal for field duplicate analyses will be plus or minus 35 percent difference (RPD) for <br /> soil samples (EPA 1988). <br /> • Field measurement (organic vapor screening, pH, conductivity, temperature) QC checks will be <br /> collected daily. Ten percent of all field measurements will be measured in duplicate. ' <br /> Table 4 lists the frequency of QA/QC samples to be collected. <br /> i <br /> Quality_Assurance_Prcject_Plan,Final.doc 5-3 - a The Source Group.Inc. <br /> r <br /> E <br />