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AL <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave -Stute 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Date <br /> ' 02 Mav-03 QC Summary Report Work Order <br /> 03042224 <br /> Method Blank Type MBLK Test Code EPA Method SW6020 <br /> File ID 042103 81025_ICB Dl Batch ID 7737 Analysis Date 04/2112403 16 37 <br /> Sample ID MB-7737 Units mg/Kg Run ID ICPIMS_030421A Prep Date 04!2112003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Htght-imit RPD Ref Val %RPD Qual <br /> Lead ND 1 <br /> tLaboratory Control Spike Type LCS Test Code EPA Method SW6020 <br /> File ID 042103 Bk026_LCS DI Batch ID 7737 Analysis Date 04/21/2003 16 41 <br /> Sample ID LCS-7737 Units mglKg Run ID ICPIMS_030421A Prep Date 0412112003 <br /> ' Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qua] <br /> Lead 26 1 25 104 85 115 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW6020 <br /> ' File ID 042103 B1029SMPL Dl Batch ID 7737 Analysis Date 04/21/2003 16 54 <br /> Sample ID 03041640-01AMS Units mg/Kg Run ID ICP/MS 030421A Prep Date 04/21/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> Lead 112 1 25 473 258 70 130 D <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW6020 <br /> File ID 042103 B1030SMPL D1 Batch ID 7737 Analysis Date 04/21/2003 16 58 <br /> ' Sample ID 03041840-01AMSD Units mg/Kg Run ID ICPIMS 030421A Prep Date 04/21/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Lead 119 1 25 473 286 70 130 1119 101 D <br /> tnenents ND-Not Detected at the Iteporting L=t D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx <br /> B-.Analyte detected in the associated Method Blank <br /> I <br /> 1 <br /> I <br />