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Alpha Analytical, Inc. p y s 255 Glendale Ave •Suite 21 •Sparks, Nevada 89431-5778 (775) 355-1044 •(775)355-0406 FAX • 1-800-283-1183 q*13 02-May 03 QC Summary Report Work Order 03042224 Method Blank Type MBLK Test Code EPA Method SW8015 File ID D IHPCHEMIMS09IDATAkO30423kO3042307 D Batch ID MS9SO423B Analysis Date 04/23/2003 11 47 ' Sample ID MBLK MS9SO4236 Units mg/Kg Run ID GCIMSD_9_030423A Prep Date 04/23/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual TPH Purgeable ND 1 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID D IHPCHEMIMS09kDATA1030423kO3042309 D Batch ID MS9SO423B Analysis Date 04/23/2003 12 34 Sample ID GLCS MS9SO423B Units mg1Kg Run!D GCIMSD_9_030423A Prep Date 0412312003 ' Analyte Result PQL SpkVal SpkRefVat %REC LowLimtt Highl-imit RPD Ref Val %RPD Qual TPH Purgeable 9 38 1 8 117 61 144 Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID D IHPCHEMIMS09kDATA1030423103042312 D Batch ID MS9SO423B Analysis Date 04/23/2003 13 46 Sample ID 03042224-02AGS Units mg/Kg Run ID GCIMSD_9_030423A Prep Date 04123/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual ' TPH Purqeable 6 63 1 8 0 83 61 144 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID 0 kHPCHEM%MS091DATAk03O423103042313 D Batch ID MS9SO423B Analysis Date 04/23/2003 14 10 ' Sample ID 03042224-02AGSD Units mg/Kg Run ID GCIMSD_9_030423A Prep Date 04/23/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual TPH Purgeable 752 1 8 0 94 61 144 6 635 12 5 Omments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank 1 i 1