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Alpha Analytical, Inc. Q 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 (775) 355-1044 •(775) 355-0406 FAX• 1-800-283-1183 61)ite QC Summary Report Work Order ' 02 Mav-03 03042224 Method Blank Type MBLK Test Code EPA Method SW8015 i File ID D kHPCHEM1MS08kDATAkO30423kO3042306 D Batch ID MSBW0423B Analysts Date 04123/2003 12 44 Sample ID MBLK MSBW0423A Units mg/L Run ID GC/MSD-8-030423A Prep Date 0412312003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual TPH Purgeable ND 005 iLaboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID D IHPCHEMIMSOB%DATAk030423103042303 D Batch ID MS8WO423B Analysis Date 0412312003 11 34 Sample 10 GLCS MSBW0423B Units mg1L Run ID GC/MSO-8-030423A Prep Date 04/23/2003 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual 1 TPH Purgeable 0 469 005 0 4 117 58 136 Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID D kHPCHEM1MS081DATA1030423kO3042310 D Batch IDMS8WO423B Analysis Date 04/23/2003 14 18 Sample ID 03042224-09AGS Units mglL Run ID GC/MSD-8-030423A Prep Date 0412312003 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual ' TPH Purcleable 2 34 025 2 0 117 58 136 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID DIHPCHEMIMS081DATA1030423103042311 D Batch ID MSSW0423B Analysis Date 04/23/2003 14 41 Sample ID 03042224-09AGSD Units mg1L Run ID GCIMSD_8_030423A Prep Date 0412312003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual TPM Purgeable 27 025 2 0 135 58 136 2 34 141 mments ND-blot Detected at the Reporting Limit D-if the spiked value is<25%of the reterence value recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx B-Analyte detected in the associated Method Blank i � i 1 i 1 ' 1 • i -