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4 Alpha Analytical Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks, Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> Date <br /> ' 02 May-03 QC Summary Report Work Order <br /> 03042224 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW82608 <br /> File ID D kHPCHEMAMS091DATAk030423103042310 D Batch ID MS9S0423A Analysis Date 04!23!2003 12 58 <br /> ' Sample ID 03042224-02AMS Units pg/Kg Run ID GC/MSD_9_030423A Prep Date 04122/2003 <br /> Analyte Result PQL SpkVai SpkRefVal %REC Lowl-imit Hight_imtt RPO Ref Val %RPD Qual <br /> 11-Dichtoroethene 151 20 200 <br /> Benzene 0 75 0 147 <br /> ' 201 5 200 0 100 60 142 <br /> Toluene <br /> Trichloroethene T 206 20 200 0 103 60 142 Chlorobenzene 206 5 200 0 103 58 143 <br /> 204 20 200 0 102 57 144 <br /> Ethylbenzene' 217 5 200 0 109 58 147 <br /> o-Xyiene ene m p- 413 5 400 0 103 57 147 <br /> en203 5 200 0 102 58 149 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> ' File ID D 1HPCHEM1MS091DATA1030423103042311 D Batch ID MS9S0423A <br /> Analysis Date 0412312003 13 22 <br /> Sample ID 03042224-02AMSD Units <br /> pg/Kg Run 1D GClM517_9_030423A Prep Date 04/22/2003 <br /> Analyte Result PQL SpkVai SpkRefVal %REC Lowl-imit Highl-emit RPD Ref Val %RPO Qual <br /> ' 1 1-Dichloroethene 128 20 200 0 64 <br /> Benzene 0 147 1507 164 <br /> 152 5 200 0 76 60 142 2007 275 <br /> Trichloroethene 159 20 200 <br /> Toluene 0 80 60 142 206 257 <br /> Chlorobenzene 158 5 200 0 79 58 143 2057 259 <br /> Ethylbenzene 157 20 200 0 79 57 144 2036 258 <br /> o-p- ne 169 5 200 0 84 58 147 2173 251 <br /> o-Xylene 324 5 400 0 81 57 147 4133 242 <br /> en <br /> 158 5 200 0 79 58 149 203 3 25 <br /> mments ND-Not Detected at the Reporting Limit D If the spiked value is<25%of the reference value recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix <br /> B-Analyte detected in the associated Method Blank <br /> 1 <br /> • <br /> 1 � <br /> i <br />