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Alpha Analytical, Inc, 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 (775) 355-1044 •(775)355-0406 FAX • 1-800-283-1183 Date Work Order ' 25-Rpr 03 QC Summary Report 03041746 Method Blank Type MBLK Test Code EPA Method SWB015 File ID D IHPCHEMIMS091DATAI030421103042108 D Batch ID MS9SO421B Analysis Date 04/21/2003 11 51 Sample ID MBLK MS9SO421B Units mg/Kg Run ID GCIMSD_9_030421A Prep Date 04/21/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLlmit Hight-imlt RPD Ref Val %RPD Qual TPH Purgeable ND 1 tLaboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID D 1HPCHEM1MS091DATA1030421103042110 D Batch ID MS9SO421B Analysis Date 04/21/2003 12 37 Sample ID GLCS MS9SO421B Units mg/Kg Run ID GC/MSD_9_030421A Prep Date 04/21/2003 ' Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hlghl-imit RPD Ref Val %RPD Qual TPH Purgeable 846 1 8 106 61 144 Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID D 1HPCHEMIMS091DATA103042lk03042119 D Batch ID�MS9SO421 B Analysis Date 04/2112003 16 05 Sample ID 03041746-02AGS Units mglKg Run ID GCIMSD 9 030421A Prep Date 04/21/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imtt Highl-imd RPD Ref Val %RPD Qua] TPH Purqeable 562 1 8 0 70 61 144 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID D 1HPCHEMIMS09IDATA1030421103042120 D Batch ID MS9SO421B Analysis Date 04/21/2003 16 29 ' Sample ID 03041746-02AGSD Units mg/Kg Run ID GCIMSD 9_030421A Prep Date 04/21/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual TPH Purgeable 641 1 8 0 80 61 144 5 619 131 omments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank 1 1 1 I