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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 Date Work Order ' 25 Apr-03 QC Summary Renort 03041746 Method Blank Type MBLK Test Code EPA Method SW8015 File ID DtiHPCHEM1MS091DATA1030418k03041806 D Batch ID MS9W0418B Analysis Date 0411612003 10 23 ' Sample lD MBLK MS9W0418B Units mglL Run ID GCIMSD_9_030418A Prep Date 04/18/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLlmlt HighLimit RPD Ref Val %RPD Qual TPH Purgeable ND 005 ' Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID D kHPCHEMkMS09%DATA%03O4lBkO3O4l8O5 D Batch ID MS9W0418B Analysis Date 04/1812003 10 00 Sample ID GLCS MS9W0418B Units mg1L Run ID GCIMSD_9_030418A Prep Date 04/18/2003 ' Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual TPH Purgeable 0 418 005 04 105 58 136 I Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID D 1HPCHEMIMS091DATA1030418k03041809 D Batch 1D_MS9W0418B Analysis Date 04/18/2003 11 34 Sample ID 03041746-10AGS Units mg/L Run lD GCIMSD 9 030418A Prep Date 04/18/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual ' TPH Purqeable 261 025 2 0 131 58 136 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 He ID D IHPCHEMIMS09%DATA1030418%03041810 D Batch ID MS9W04188 Analysis Date 04118/2003 11 57 ' Sample ID 03041746-10AGSD Units mg1L Run lD GC/MSD-9-030418A Prep Date 04/1812003 Analyte Result PQL SpkVal SpkRe(Val %REC Lowl-imlt HighLimit RPD Ref Val %RPD Qual TPH Purgeable 2 38 025 2 0 119 58 136 2 613 9 34 I—on,ments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank t I •