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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Service Request: S9901001 <br /> Project: Teichert&Sons-Stockton/20F90-002.007 Date Collected: NA <br /> Sample Matrix: Soil Date Received: NA <br /> Fuel Oxygenates <br /> Sample Name: Method Blank Units: ug/Kg(ppb) <br /> Lab Code: 5990402-SBI Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRI. Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 500 1 4/2/99 4/2/99 ND <br /> Methyl tert-Butyl Ether NONE 8260 5 1 4/2/99 4/2/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> Page 15 <br />