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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Service Request: 59901001 <br /> Project: Teichert&Son s-S tockton/20F90-002.007 Date Collected: 3/23 -3/24/99 <br /> Sample Matrix: Soil Date Received: 3/25/99 <br /> TPH as Diesel <br /> Prep Method: LOFT Units: mg/Kg(ppm) <br /> Analysis Method: California DHS LUFT Basis: Wet <br /> Test Notes: <br /> Dilution Date Date Result <br /> Sample Name Lab Code MRI, Factor Extracted Analyzed Result Notes <br /> SP-1A/B S9901001-025 1 1 4/2/99 4/3199 12 <br /> SP-2A/B S9901001-026 1 1 4/2/99 4/3/99 440 <br /> SP-3AB S9901001-027 1 1 4/2/99 4/3/99 190 D5 <br /> SP-4A/B 59901001-028 1 1 412/99 4/5/99 820 <br /> SP-5AB 59901001-029 1 1 4/2199 4/3199 130 <br /> SP-6A/B S9901001-030 1 1 4/2/99 4/5/99 100 <br /> SP-7A/B S9901001-031 1 1 4/2/99 4/3/99 200 <br /> SP-8A/B S9901001-032 1 l 4/2/99 4/5/99 340 D5 <br /> SP-9AB 59901001-033 1 1 4/2/99 4/5/99 130 D5 <br /> SP-IOA/B S9901001-034 1 1 4/2/99 413/99 52 <br /> SP-IIA/B 59901001-035 1 1 4/2199 4/5/99 95 D2 <br /> SP-12A/B 59901001-036 1 1 4/2/99 4/5/99 240 <br /> Method Blank 5990402-SBI 1 1 4/2199 4/3/99 ND <br /> D2 The sample contains a higher boiling point hydrocarbon mixture quantitated diesel. The <br /> chromatogram does not match the typical diesel fingerprint. <br /> D5 The sample contains a higher boiling point mixture of hydrocarbons and diesel quantitated as diesel. <br /> IA1020597p <br /> Page 16 <br />