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i <br /> Analytical Laboratory 56 of 61 <br /> CERTIFICATE OFANAL YSIS <br /> Tues October 18,2005 <br /> Attention Jack Bishop <br /> California Tank Lines <br /> Report Page 18 of 22 <br /> P O BOX 6245 <br /> Stockton, CA 95206 <br /> i <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Precision Enviro-Tech <br /> Reporting Spike Source %REC RPD <br /> �Amlyte Result Limit Units Level Result °/,REC Limits RPD Limit Notes <br /> Batch AI51405-Volatiles <br /> Blank(AI51405-BLKI) Prepared&Analyzed 14-Sep-05 <br /> tert-Butyl Acohol(TBA) ND 500 no <br /> Methyl tert-butyl Ether(MTBE) ND 0 500 " <br /> Dimpropyl Ether(DIPE) ND 0 500 " <br /> Ethyl tert Butyl Ether(ETRE) ND 0 500 " <br /> tert Amy]Methyl Ether(TAME) ND 0 500 " <br /> 1,2-Dibromoethane(EDB) ND 0 500 " <br /> 12-Dichloroetime ND 0500 " <br /> Benzene ND 0 500 " <br /> Ethylbenzene ND 0 500 " <br /> Toluene ND 0 500 " <br /> wyXylen <br /> ND 0 500 <br /> lene ND 0 500 <br /> LCS(AI51405-BSI) Prepared&Analyzed 14-Sep-05 <br /> tert Butyl Acohol(TBA) 102 Soo ugA 100 102 75 122 <br /> Methyl ted-butyl Ether(MtBE) 490 0 500 400 120 75-122 <br /> Dusopropyl Ether(DIPE) 220 0 500 200 110 75-122 <br /> Ethyl tert Butyl Ether(ETRE) 201 0 500 200 100 75 122 <br /> tert-Amyl Methyl Ether(TAME) 194 0 500 200 97 75 122 <br /> 1,2 Dibromcethane(EDB) 190 0 500 200 95 75 122 <br /> 12 Dichloroethane 18 5 0 500 200 92 75 122 <br /> Benzene ISO 0 500 200 90 75-122 <br /> Ethylbenzene 163 0 500 200 82 75-122 <br /> Toluene 210 0 500 200 105 75-122 <br /> in p-Xylene 420 0 500 400 105 75 122 <br /> *-Xylene ISO 0 500 200 90 75 122 <br /> Matna Spike(AI51405-MS1) Source 5091410-03 Prepared 14-Sep-05 Analyzed 15-Sep-05 <br /> tert-Butyl Acohol(TBA) 102 500 ug/I t00 ND 102 75-122 <br /> Methyl tent butyl Ether(MtBE) 420 0 500 400 ND 105 75-122 <br /> Diisopropyl Ether(DIPE) ISO 0 500 200 ND 90 75-122 <br /> Ethyl Cert Butyl Ether(ETRE) 210 0 500 200 ND 105 75 122 <br /> tert Amyl Methyl Ether(TAME) 191 0 500 200 ND 96 75 122 <br /> 1 2-Dibromoethane(EDB) 178 0 500 200 ND 89 75 122 <br /> mg,L-mdhgrams per Laer=ppm DLR-Detecnrm Lrmrtf—Pu pse of ftornng <br /> ag/L--rog—perLrter=ppb Ereep[ianal sample mamces or interferences may <br /> result in higher detectiarr hmits <br /> RESPECTFULLY SUBMITTED, <br /> *��/Ow� <br /> Jonathan Le,Laboratory Director <br /> j743.N Rest Lane Suate B2 Stockton CA 95210 nhone (209) 477-8105 Fac (209) 477-8148 <br />