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Analytical Laboratory 57 of 61 <br /> _ CERTIFICATE OF ANALYSIS <br /> Tuesday, October 18,2005 <br /> Attention Jack Bishop <br /> California Tank Lines RemnPage 19 of 22 <br /> P O BOX 6245 <br /> Stockton,CA 95206 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Precision Enviro-Tech <br /> Reporting Spice Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Lmuts RPD Limit Notes <br /> Batch AI51405-Volatiles <br /> Matnx Spike(AI51405-MSI) Source 5091410-03 Prepared 14-Sep-05 Analyzed 15-Sep-05 <br /> 1 2-Dichloroethane 204 0 500 U911 200 ND 102 75-122 <br /> Benzene 202 0 500 " 200 ND 101 75 122 <br /> Ethylbenzene 190 0 500 " 200 ND 95 75-122 <br /> Toluene 192 0 500 200 ND 96 75 122 <br /> in p.Xylene 390 0 500 " 400 ND 95 75 122 <br /> o-Xylene 167 0 500 200 ND 84 75 122 <br /> Matrix Spike Dup(A151405-MSDI) Source 5091410-03 Prepared 14-Sep-05 Analyzed 15-Sep-05 <br /> tert-Butyl Acahal(IBA) 101 500 ugll 100 ND 101 75-122 1 15 <br /> Methyl tent butyl Ether(MtBE) 420 0 500 400 ND 105 75-122 0 15 <br /> Dnsopropyl Ether(DIPE) 180 0 500 200 ND 90 75-122 0 15 <br /> y]tert Butyl Ether(ETBE) 195 0 500 200 ND 98 75-122 7 15 <br /> Amyl Methyl Ether(TAME) 172 0 500 200 ND 86 75-122 10 15 <br /> 1 2-Dibromoethane(EDB) 165 0 500 200 ND 82 75-122 8 15 <br /> l 2-Dichloroethane 184 0 500 200 ND 92 75-122 10 15 <br /> Benzene 184 0 500 200 ND 92 75-122 9 15 <br /> Ethylbenzene 187 0 500 200 ND 94 75-122 2 15 <br /> Toluene 192 0 500 200 ND 96 75-122 0 15 <br /> m p-Xylene 410 0 500 400 ND 102 75-122 8 15 <br /> o-Xylene 188 0 500 200 ND 94 75-122 12 15 <br /> � I <br /> I <br /> mg,L—milligrams per Luer=ppm DLR—D efechon Lrmajor Purpose ofReporhng <br /> ug,L—micrograms per tiler=ppb Escephonul sample mainces or mferkrences may <br /> resuil to higherdefecual hmits, <br /> RESPECTFULLY SUBMITTED, <br /> ole'��/Otr� <br /> Jonathan Le,Laboratory Director <br /> 7-143 Ar Nest Lane Suite B2 Stockton C4 95210 nhone (2091 477-8105 Fax (209) 477-8148 <br />