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i <br /> 110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> WCAlMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http 1/www mccampbell corn E-mail main@mccampbell corn <br /> ' Advanced GeoEnvironmental Client Project ID Pacific Pnde/S El ! Date Sampled 12l20/01 <br /> 837 Shaw Road Dorado Date Received 12/21/01 <br /> Stockton, CA 95215 Client Contact Tien.Cuellar Date Extracted 12131-01/04102 <br /> Chent P 0 Date Analyzed 12/31-01/04/02 <br /> ' Seven Oxygenated Volatile Organtes By GC/MS <br /> EPA method 3260 modified <br /> Lab ID 87271 87272 87273 87274 <br /> MWI/ MW2/ MW3/ MW4/ Reporting Linnt <br /> Client ID 12-20-01 12-20-01 12-20-01 12-20-01 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg + uglL <br /> Di-isopropyl Ether(D1PE) ND<5 0 ND + ND ND 50 10 <br /> I i <br /> Ethyl tert-Butyl Ether(ETBE) ND<5 0 ND ND ND 5 0 10 <br /> Methyl tent-Butyl Ether(MTBE) 27 ND ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<5 0 ND ND ND 5 0 10 <br /> ' tert-Butanol 230 ND ND ND 25 5 0 <br /> Methanol ND<2500 ND ND ND 2500 500 <br /> Ethanol ND<250 ND ND ND 250 50 + <br /> Surrogate Recoveries(%) <br /> Dtbromofluoromethane 95 106 106 113 <br /> 1 Comments <br /> *water samples are reported to uglL,soil and sludge samples in ug/kg,wipes m ug/wtpe and all TCLP I STLC/SPLP extracts m ug/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analvsis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment 0)sample diluted due to <br /> high organo content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />