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it110_nd avenue South #D7,Pac.'ieco CA 91553-5560 <br /> McCANDBELL ANALYTICAL INC Telepnone 925-79S-1620 Fax 925-798-1622 <br /> ' http//www mccamp bell com E-mail main@mccamobell cotta <br /> ' Advanced GeaEnvnonmental Client Pro]ecI ID Pacific Pride/S El <br /> Date Sampled 12/20/01 <br /> Dorado Date Received 12/21/01 <br /> 837 Shaw Road <br /> Stockton, CA 95215 Client Contact Tina Cuellar Date Extracted 12/31-01/04/02 <br /> Client P O Date Analyzed 12131-01/04/02 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 87275 87276 87277 <br /> ' MW51 MW6/ MW7/ Reporting Limit <br /> Client ID 12-20-01 12-20-01 12-20-01 <br /> Matrix W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND<25 50 1 0 <br /> I <br /> Ethyl tent-Butyl Ether(ETBE) ND ND ND<25 50 1 0 <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND<25 50 to <br /> i <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<25 50 1 0 <br /> ' tert-Butanol ND ND ND<125 25 50 <br /> Methanol ND ND ND<12,500 2500 500 <br /> 1 <br /> Ethanol ND ND ND<1250 250 50 <br /> Surrogate Recoveries{%) <br /> Dibromo fluoromethane 113 113 101 <br /> ' Comments 7 <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 11 Edward Hamilton,Lab Director <br />