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' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmentai Inc Client Project ID Pacific Pride-West Lane Sampled 10-09-03 <br />' of Northern California Reference Number 6211 Received 10-14-03 <br /> 837 Shaw Road Sample Description Soil Extracted 10-15-03 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-17-03 <br /> Attn Tim Cuellar Lab Numbers 6211-1S 2S 3S,4S, 5S Reported 10-30-03 <br />' GASOLINE ADDITIVES BY EPA METHOD 8260 GUMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE 1D SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT P8-5 P8-10 P8-20 P8-35 P8-45 <br /> (m /K (m /K m /K } (mg/Kg ) (m /Kg) (mg/Kg) <br /> FUEL OXYGENATES <br />' Methyl tert-Butyl Ether(MTBE) 0 010 NO NO ND NO NO <br /> Di-isopropyl Ether (DIPS) 0 010 NO NO NO NO NO <br />' Ethyl tert-Butyl Ether (ETBE) 0 010 NO NO NO NO NO <br /> tert-Amyl Methyl Ether(TAME) 0 010 ND NO ND NO NO <br />' tert-Butanol(TBA) 0 800 NO NO NO NO ND <br />' VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1,2-DCA) 0 010 NO NO NO NO ND <br />' Ethylene Dibromide (EDB) 0 010 NO NO ND NO ND <br /> Report Limit Multiplication Factor 1 1 1 1 1 <br /> I <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 607% 678% 912% 656% 786% <br /> Toluene-d8 448% 640% 712% 631% 629% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> ImglKg = milligra per kdogra or parts per million(ppm) <br /> . ANALYST APPROVED Bya <br /> Clan J Cone hillips <br /> Director <br /> I <br />