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1 <br />' CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive,Atwater CA 95301 Phone (209) 384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvlronmental Inc Client Protect ID Pacific Pride-West Lame Sampled 10-09-03 <br />' of Northern California Reference Number 6211 Received 10-14-03 <br /> 837 Shaw Road Sample Description Sod Extracted 10-15-03 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-17-03 <br /> Attn Tim Cuellar Lab Numbers 6211-6S 7S,8S, 9S, 10S Reported 10-30-03 <br />' GASOLINE ADDITIVES BY EPA METHOD 8260 GCIMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT P9-5 P9-15 P9-25 P9-40 P9-50 <br /> (ma/Ka) (m /K } mIK ) (mg/K2) (mg/Kg) (mg/Kg) <br /> FUEL OXYGENATES <br /> IMethyl tert-Butyl Ether(MTBE) 0 010 NO NO 0 059 NO ND <br /> Di-isopropyl Ether (DIPS) 0 010 NO NO NO ND ND <br /> Ethyl tert-Butyl Ether (ETRE) 0 010 NO ND ND NO ND <br /> tert-Amyl Methyl Ether(TAME) 0 010 NO NO NO NO ND <br />' tert-Butanol(TBA) 0 800 NO ND ND ND NO <br /> VOLATILE HALOCAR ONS <br /> I 1 2-Dichloroethane (1 2-DCA) 0 010 ND ND NO NO NO <br /> Ethylene Dibromide (EDB) 0 010 ND NO ND ND ND <br /> Report Limit Multiplication Factor 1 1 1 1 1 <br /> I <br /> ISurrogate Recoveries <br /> 1 2-Dichloroethane-d4 596% 896% 784% 720% 793% <br /> Toluene-d8 470% 710% 623% 583% 59911/6 <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligrams per 3cslogram or parts per million(ppm) <br /> I <br /> . ANALYST �l i /l/� APPROVED BY ' <br /> I Clair J Cone l'iaboratory <br /> es <br /> hrllrps <br /> Director <br /> 1 <br />