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1 <br />' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209) 384-2930 <br />' Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnviron mental, Inc Client Project ID Pacific Pride-West Lane Sampled 10-10-03 <br />' of Northern California Reference Number 6212 Received 10-14-03 <br /> 837 Shaw Road Sample Description Soil Extracted 10-15-03 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-17-03 <br /> Atin Tim Cuellar Lab Numbers 6212-1S 2S 3S,4S 5S Reported 10-30-03 <br /> 1 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GC/MS <br /> 1 <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT P11 - 15 P11 -25 P11 -35 P11 -45 P12-15 <br /> (m /K ) m /K (m /K ) (mg/Kg)--- (m !K ) rn IK ) <br /> FUEL OXYGENATES <br />' Methyl tert-Butyl Ether(MTBE) 0 010 ND ND ND ND 014 <br /> Di-isopropyl Ether (DIPE) 0 010 ND ND ND ND ND <br />' Ethyl tert-Butyl Ether (ETRE) 0 010 ND ND ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 010 NO ND ND ND ND <br /> tert-Butanol(TBA) 0 800 ND` ND ND ND ND <br />' VOLATILE HALOCARBONS <br /> 12-Dichloroethane (1,2-DCA) 0010 ND ND ND NO ND <br />' Ethylene Dibromide (ED6) 0 010 ND ND NO ND ND <br /> Report Limit Multiplication Factor 1 1 1 1 1 <br /> I <br /> I Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 837% 984% 831% 665% 673% <br /> Toluene-d8 703% 906% 81 8% 641% 608% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligrams-per kilogram arts per million(ppm) <br /> ANALYST APPROVED B <br />' Clair J Cane aarnehillips <br /> Laboratory Director <br />