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' CASTLE ANALYTICAL LABORATORY <br /> • Environmental Testing Services 2333 Shuttle Drive Atwater,CA 95301 Phone (209)384-2930 <br />' Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmentaf Inc Client Project ID Pacific Pride-West Lane Sampted 10-10-03 <br />' of Northern California Reference Number 6212 Received 10-14-03 <br /> 837 Shaw Road Sample Description Sod Extracted 10-15-03 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-17-03 <br /> Attn Trm Cuellar Lab Numbers 6212-6S, 7S,8S Reported 10-30-03 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GC/MS <br />' ANALYTE REPORTING SAMPLE ID SAMPLE ID <br /> SAMPLE ID <br />' LIMIT P12-25 P12-40 P12-50 <br /> (m /K m /K ) (m IK m /K <br /> FUEL OXYGENATES <br />' Methyl tort-Butyl Ether(MTBE) 0 010 ND ND NO <br /> Di-isopropyl Ether (DIPE) 0 010 ND NO NO <br />' Ethyl tert-Butyl Ether (ETBE) 0 010 ND NO ND <br /> tert-Amyl Methyl Ether(TAME) 0 010 NO ND NO <br />' tert-Butanol (TBA) 0 800 ND NO NO <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1 2-DCA) 0 010 ND NO NO <br /> Ethylene Dibromide (EDB) 0 010 NO NO ND <br /> Report Limrt Multiplication Factor 1 1 1 <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 822% 563% 71 6% <br /> Toluene-d8 893% 493% 598% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligra per kdogra r parts per million(ppm) <br /> I r <br /> ANALYST APPROVED BY <br /> Clan J Cone Ja s C rlhps <br /> boratory Director <br /> I <br />