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Amcricur7. E ,ii-nrr miacll Netwoi- <br /> WORK ORDER: 9712299 QUALITY CONTROL REPORT PAGE QR-2 <br /> SANALYSIS: Gasoline Oxygenates <br /> MATRIX: Water <br /> METHOD BLANK SAMPLES <br /> ..........--................................................................................................................. <br /> SAMPLE TYPE: Blank-Method/Media blank LAB ID: BLNK_1229 INSTR RUN: GCMS13\911229000000/1/ <br /> INSTRUMENT, HP mass spec for Volatiles PREPARED: BATCH ID: MS13WI23097 <br /> UNITS: ug/L ANALYZED: 12/29/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1.2-DCE-d4 (surr) 86.2 100 100 86.2 70 130 <br /> Toluene-d8 (surr) 103 100 100 103 70 130 <br /> Bromofluorobenzene (surr) 78.9 100 100 78.9 70 130 <br /> Methy-t-butyl ether (MTBE) ND 5 <br /> Ethyl-t-butyl ether (ETRE) NO 5 <br /> t•Amylmethyl ether (TAME) ND 5 <br /> t-Butanol (TBA) ND 100 <br /> Di-isopropyl ether (DIPS) NO 5 <br /> LABORATORY CONTROL SAMPLES <br /> ------------••--------------------••------------•---------------------------------------------•-----------•-----•. .......... <br /> SAMPLE TYPE: Laboratory Control Spike LAB ID: LCSW_1229 INSTR RUN: GCMS13\971229000000/2/1 <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 <br /> UNITS: ug/L. ANALYZED: 12/29/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1.2-DCE-d4 (surr) 94.8 86.2 100 100 94.8 70 130 <br /> Toluene-d8 (surr) 103 103 100 100 103 70 130 <br /> Bromofluorobenzene (surr) 76.9 78.9 100 100 76.9 70 130 <br /> Methy-t-butyl ether (MTBE) 122 ND 5 100 122 32 158 <br /> Ethyl-t-butyl ether (ETBE) 142 ND 5 100 142 32 158 <br /> t-Amylmethyl ether (TAME) 101 ND 5 100 101 32 158 <br /> -------------•-----------•--------••-------•--•--------...---------•--•----- ................................................ <br /> MATRIX SPIKE SAMPLES <br /> ----------• --------------------------•-------------•---------••--------•-------....------------.....--------•----•---------- <br /> SAMPLE TYPE: Spike-Sample/Matrix LAB ID: MD12299-01D INSTR RUN: GCMS13\971229000000/11/4 <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 <br /> UNITS: ug/L ANALYZED: 12/30/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (%) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1.2-DCE•d4 (surr) 92.4 85.2 100 100 92.4 70 130 <br /> Toluene-d8 (surr) 95.6 96.0 100 100 95.6 70 130 <br /> Bromofluorobenzene (surr) 87.5 85.2 100 100 87.5 70 130 <br /> Methy-t-butyl ether (MTBE) 111 ND 5 100 111 32 158 <br /> Ethyl-t-butyl ether (ETRE) 122 ND 5 100 122 32 158 <br /> t-Amylmethyl ether (TAME) 101 ND 5 100 101 32 158 <br /> -------------------------...................................................................--------------................... <br /> SAMPLE TYPE: Spike-Sample/Matrix LAB ID: NS12299-01D INSTR RUN: GCMS13\911229000000/10/4 <br /> INSTRUMENT. HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 <br /> UNITS: ug/L ANALYZED: 12/30/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1,2-DCE-d4 (surr) 94.1 85.2 100 100 94.1 70 130 <br /> Toluene-d8 (surr) 101 96.0 100 100 101 70 130 <br /> Bromofluorobenzene (surr) 87.2 85.2 100 100 87.2 70 130 <br /> Methy-t-butyl ether (MTBE) 109 NO 5 100 109 32 158 <br /> Ethyl-t:butyl ether (£TBE) 120 - NO 5 100 120 32 158 <br /> t-Amylmethyl ether (TAME) 100 NO 5 100 100 32 158 <br />