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American Eiiviroiwiewal Network WORK ORDER: 9712299 QUALITY CONTROL REPORT PAGE QR-3 ANALYSIS: Gasoline Oxygenates MATRIX: Waiver MATRIX SPIKE DUPLICATES ----------------------------------------•--...-----•------------------------------------------------------•------------•- SAMPLE TYPE: Spiked Sample Duplicate LAB ID: MR12299-OID INSTR RUN: GCMS13\971229000000/12/10 INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 UNITS: ug/L ANALYZED: 12/30/97 DILUTION: 1.00 METHOD: REF REPORTING SPIKE RECOVERY REC. LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1.2-ACE-d4 (surr) 92.4 94.1 100 100 92.4 70 130 Toluene-d8 (surr) 95.6 101 100 100 95.6 70 130 Bromofluorobenzene (surr) 87.5 87.2 100 100 87.5 70 130 Methy-t-butyl ether (MTBE) 111 109 5 1.82 25 Ethyl-t-butyl ether (ETBE) 122 120 5 1.65 25 t-Amylmethyl ether (TAME) 101 100 5 0.995 25 t-Butanol (TBA) ND NO 100 0 Di-isopropyl ether (DIPS) ND NO 5 0 ....-•-•-•-•------------------------------------------------------------------------•---•--...------------------••-- SAMPLE SURROGATES --------------------- ...................................---................................................................. SAMPLE TYPE: Sample-Client LAB ID: 9712299.01D INSTR RUN: GCMS13\971229000000/4/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 UNITS: ug/L ANALYZED: 12/29/97 DILUTION: 1.00 METHOD: REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1.2-DCE-d4 (surr) 85.2 100 100 85.2 70 130 Toluene-d8 (surr) 96.0 100 100 96.0 70 130 Bromofluorobenzene (surr) 85.2 100 100 85.2 70 130 ............................................................................................................................. ..------•---------------•----------------------------------------------...................--------------------------- SAMPLE TYPE: Sample-Client LAB ID: 9712299-02D INSTR RUN: GCMS13\971229000000/5/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 UNITS: ug/L ANALYZED: 12/29/97 DILUTION: 1.00 METHOD: REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD _ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1,2-DCE-d4 (surr) 91.4 100 100 91.4 70 130 Toluene-d8 (surr) 100 100 100 100 70 130 Bromofluorobenzene (surr) 86.8 100 100 86.8 70 130 -•------------------------------------------•-----------------------.......----------------------------------- --------- SAMPLE TYPE: Sample-Client LAB ID: 9712299-03D INSTR RUN: GCMS13\971229000000/6/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13WI23097 UNITS: ug/L ANALYZED: 12/29/97 DILUTION: 1.00 METHOD: REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1,2-DCE-d4 (surr) 88.5 100 100 88.5 70 130 Toluene-d8 (surr) 101 100 100 101 70 130 Bromofluorobenzene (surr) 87.0 100 100 87.0 70 130 -----------------------------•---------•-----------------------------------•--------------------•------------....------------ SAMPLE TYPE: Sample-Client LAB 10: 9712299-04D INSTR RUN: GCMS13\971229000000/7/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W123097 UNITS: ug/L ANALYZED: 12/29/97 DILUTION: 1.00 METHOD: REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1,2-OCE-d4 (surr) 91.6 100 100 91.6 70 130 Toluene-d8 (surr) 101 100 100 101 70 130 Bromofluorobenzene (surr) 85.6 100 100 85.6 70 130 --------------------------------------------------- --------------------------------------------- .................... ---------