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REG 603 UPDATE-9 9/14/92 <br /> E prior to a filter in front of the vacuum pump. After the vapor <br /> stream leaves the vacuum pump, it is pushed into the thermal <br /> oxidizer (RXL 400 ) which oxidizes the gasoline range hydrocarbon <br /> vapors at no less than 1400OF and no greater than 1550121F! <br /> Influent samples are obtained from the exit of the pump and <br /> effluent samples are obtained from the stack of the thermal] <br /> oxidizer . The gasoline range hydrocarbons are oxidized into heat, <br /> CO2 and water vapor, see UPDATE STATUS REPORT #5 . <br /> f <br /> A portable ambient air PID-GC (Photovac 10550 packed column) is <br /> used at the site to sample the influent and effluent of the REMOX <br /> i oxidizer , and the individual wells (MW1 , MW2-3 , MW10 and EX-411 ) , <br /> see Tables 2 , and 3 . on October 22 , and 24 , 1991 , "Tedlar" bag <br /> samples were obtained of the influent and effluent of the REMOX <br /> incenerator and on January 20 , May 21 , June 22 , July 15 , and <br /> August 26 , 1992, a influent sample was obtained. These samples <br /> were analyzed for TFH and BTEX along with screening for <br /> Tetrachloroethylene (PCE) , Trichloroethylene (TCE) and 1 ,2 ,- <br /> Dichloroethane (DCE) using a Shimadzu GC-FID chromatograph mounted <br /> permanently in WEGE's portable laboratory. These compounds have <br /> the following retention times in the above chromatograph, DCE = <br /> 2. 079 minutes , TCE = 3 .023 minutes and PCE = 3 . 75 minutes . Prior <br />. to sampling the wells or the system, a calibrant prepared from <br /> fresh gasoline is injected into the GC-PID. The resulting <br /> chromatogram has numerous responses . The microprocessor of the <br /> GC-PID computes the area, per response, in volt seconds , and <br /> assigns a peak # , and retention time. The sum of all the <br /> responses are then used to obtain a mg/L per volt second calibrant <br /> factor , which is used to calculate mg/L as gasoline vapor from <br /> each analysis produced. Pounds per day can be computed using <br /> these mg/L values produced from the anlaysis of the different <br /> vapor recovery wells and the influent to the oxidizer , and the <br /> pressure differential created at the orifice to determine flow <br /> rates for each well and the influent to the oxidizer. The pounds <br /> per day values for each well and the influent are then averaged <br /> with the preceeding site visits pound per day value and then <br /> multiplied by the number of days the system operated between <br /> visits to estimate the total pounds each well and the system has <br /> removed for that time period. This poundage is then added to the <br /> accumulated poundage of the previous visit to update the total <br /> pounds removed to date. The effluent sample is computed in the <br /> same fashion, but also includes natural gas flow along with the <br /> I influent orifice flow rate. <br /> SAMPLING VAPOR STREAMS <br /> The vapor samples are obtained by attaching a dedicated air tight <br /> 60 cc syringe to a sample port on the vapor recovery manifold, <br />. i well side of the orifice plate, with air tight fitted polytubing . <br /> PAGE 6 <br /> i <br />