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S U R R O G A T E R E COYER 1 E S R E P O R T Job Number 992708 Report Date 01/06/2000 CUSTOMER IT Group PROJECT Southland - Martinez ATTN Rhonda Teicheira Method Volatile Organics by GC/MS Batch 10411 Method Code 8260OX Analyst gfb Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 992648-1 Solid 1 26 37 25 000 105 5 60-160 12/27/1999 0338 992648 1 Solid MS 26 11 25 000 104 4 60-160 12/27/1999 0730 992648-1 Solid MSD 25 45 25 000 101 8 60-160 12/27/1999 0803 992691-8 Liquids 1 25 60 25 000 102 4 57-162 12/29/1999 0331 992691-9 Liquids 1 25 16 25 000 100 6 57-162 12/29/1999 0414 992712 2 Liquids 1 25 06 25 000 100 2 57-162 12/29/1999 0447 992691-4 Liquids 2 24 65 25 000 98 6 57-162 12/29/1999 0520 992691-7 Liquids 4 24 74 25 000 99 0 57-162 12/29/1999 0700 992712 2 Liquids MS 24 18 25 000 96 7 57-162 12/29/1999 0733 992712-2 Liquids MSD 25 11 25 000 100 4 57-162 12/29/1999 08D5 691-5 liquids 200 25 74 25 000 103 0 57-162 12/29/1999 0839 91 6 Liquids 2 24 12 25 000 96 5 57-162 12/29/1999 0912 08 3 Solid 1 26 82 25 000 107 3 60-160 12/29/1999 0945 LCS 1 24 69 25 000 98 8 57-162 12/29/1999 1139 MB 1 25 52 25 000 102 1 57-162 12/29/1999 1213 992691 3 Liquids 2 25 42 25 000 101 7 57-162 12/29/1999 1246 Method Volatile Organics -Aromatics Batch 10428 Method Code 8020BX Analyst evd Surrogate, Units 1 4-Bromafluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time LCS 1 41 45 50 0000 82 9 64-147 01/04/2000 1642 LCD 1 43 19 50.0000 86 4 64-147 01/04/2000 1708 MB 1 40 98 50 0000 82 0 64-147 01/04/2000 1800 992709-4 Solid MS 1 44 45 50 0000 88 9 64-147 01/04/2000 1944 992709-4 Solid MSD 1 41 81 50 0000 83 6 64-147 01/04/2000 2010 992693 7 Solid 1 41 16 50 0000 82 3 64-147 01/04/2000 2036 992693-11 Solid 1 39 76 50 0000 79 5 64-147 01/04/2000 2128 992693-12 Solid 1 41 49 50 0000 83 0 64-147 01/04/2000 2153 992693-14 Solid 1 42 98 50 0000 86 0 64-147 01/04/2000 2219 992693 40 Solid 1 40 51 50 0000 81 0 64-147 01/04/2000 2245 I 992693 45 Solid 1 40 27 50 0000 80 5 64 147 01/04/2000 '2311 992693-48 Solid 1 38 85 50 0000 77 7 64 147 01/04/2000 2337 992693 52 Solid 1 40 99 50 0000 82 0 64-147 01/05/2000 0002 1992709 3 Solid 1 40 92 50 0000 81 8 64-147 01/05/2000 0211 992709-4 Solid 1 32 34 50 0000 64 7 64-147 01/05/200010821 #708=3Solid 1 33 11 50 0000 66 2 64-147 01/05/2000 0939 08-4 Solid 1 34 56 50 0000 69 1 64-147 01/05/2000 1004 05-3 Solid 1 35 81 50 0000' 71 6 64 147 01/05/2000 1030 992705=5 Solid 1 37 07 510 0000 74 1 64 147 01/05/2000 1232 Page � I II III I I r II 1 , rl r I E�, I I {{ t I E 111 rfl I' EI rll ISI I 1f11 li CI 1 II ri Iv 5�`t dl II