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S U R R O G A T E R E C O V E R I E S R E P O R T Job Number 992708 Report Date 01/06/2000 CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheera Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 992707-3 Solid 1 35 85 50 0000 71 7 64-147 01/05/2000 1258 Method Volatile Organics by GC/MS Batch 10443 Method Code 8260OX Analyst gfb Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 56-6 Soled 1 23 48 25 000 93 9 60-160 12/07/1999 1442 56-6 Solid MS 23 57 25 000 94 3 60-160 12/07/1999 1705 56-6 Solid MSD 24 61 25 000 98 4 60-160 12/07/1999 1740 992636-2 Liquids MS 24 66 25 000 98 6 57-162 12/24/1999 0225 992636-2 Liquids MSD 24 24 25 000 97 0 57-162 12/24/1999 0259 992704-1 Liquids 1 25 01 25 000 100 0 57-162 01/04/2000 0103 992704-2 Liquids 1 24 70 25 000 98 8 57-162 01/04/2000 0136 992704-3 Liquids 1 25 36 25 000 101 4 57-162 01/04/2000 0208 992704-4 Liquids 1 25 04 25 000 100 2 57-162 01/04/2000 0241 LCS 1 25 42 25 000 101 7 57-162 01/04/2000 0636 MB 1 25 51 25 000 102 0 57-162 01/04/2000 0742 992709-8 Solid 1 25 00 25 000 100 0 60-160 01/04/2000 0814 992712-1 Solid 1 26 89 25 000 107 6 60-160 01/04/2000 0847 992712-3 Solid 1 24 87 25 000 99 5 60-160 01/04/2000 0919 992705-3 Soled 1 25 43 25 000 101 7 60-160 01/04/2000 0952 992705-4 Solid 1 23 74 25 000 95 0 60-160 01/04/2000 1024 992705-5 Solid 1 24 70 25 000 98 8 60-160 01/04/2000 1056 CV 1 25 60 25 000 102 4 57-162 01/04/2000 1155 992708-4 Soled 1 26 79 25 000 107 2 60-160 01/04/2000 1230 992636-2 Liquids 1 25 43 25 000 101 7 57-162 12/23/2099 0952 I i 1 r r I I I i i I I I Page 11 I I. h- I I li