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Q UAL I T Y C O N T R O L R E 5 U L T 5 <br /> Job Number 992709 Report Date 01/06/2000 <br /> CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheira <br /> QC Type Description Reag Code Lab [D Dilution Factor Date Time <br /> MB Method Stank 12/31/2099 0236 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> itert-ButyL Alcohol (TBA) 0 <br /> Di-Isopropyl Ether _ 1 32 <br /> Ethyl tert-Butyl Ether (ETBE) 0 <br /> Cert-Amyl Methyl Ether 0 <br /> �Methyl-t-Butyl Ether (MTBE) (I <br /> 1,2-Dichloroethane 0 <br /> 1,2-Dibromoethane (EDB) 0 <br /> Test Methad EPA 8260B Batch 10443 Analyst gfb <br /> Method Description Volatile Organics by GC/MS Units ug/L <br /> MS Matrix Spike 09112901 992556-6 12/07/1999 1705 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> Butyl Alcohol (TBA} 1317 66 100D.000000 0 131 8 48-194 <br /> opropyl Ether 38 89 50 000000 0 77 8 53-149 <br /> Ethyl tert-Butyl Ether (ETBE) 43 21 50 000000 0 85 4 53-148 <br /> tert-Amyl Methyl Ether 42 90 50.000000 0 85 8 49 158 <br /> Methyl-t-Butyl Ether (MTBE) 111 38 100 000000 0 43 111 0 44-190 <br /> �1,2-Dichloroethane 11 04 10 000000 0 110 4 70-130 <br /> 1,2-Dibromoethane (EDB) 8 29 10 000000 0 82 9 70-130 <br /> MSD Matrix Spike Duplicate 09112901 992556-6 :1 1 12/07/1999 1740 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 1036 41 1317 66 1000 000000 0 103 6 48-194 <br /> 24 21 Y <br /> Di-Isopropyl Ether 32 89 38 89 50 000000 0 65 8 53-149 <br /> 17 15 Y <br /> Ethyl tert-Butyl Ether (ETBE) 35 82 43 21 50 000000 0 71 6 53-148 <br /> 19 28 <br /> r Cert-Amyl Methyl Ether 36 71 42 90 50 000000 0 73 4 49-158 <br /> 16 48 <br /> Methyl-t-Butyl Ether (MTBE) 94 50 111 38 100 000000 0 43 94 1 44-190 <br /> 16 21 <br /> �1,2-6ichloroethane 9 97 11 04 10 000000 0 99 7 70-130 <br /> 10 30 <br /> 1,2-Dibromoethane (EDB) 6 17 8 29 10 000000 0 61 7 70-130 X <br /> 29 30 <br /> 1 <br /> MS Matrix Spike 0!120705 !l263i-2 12/x4/1999 0225 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> t Butyl Alcohol (TBA) 1161 58 1000 000000 1 80 116 0 34-182 <br /> .propyl Ether 61 54 50 000000 0 123 1 60-131 <br /> L Cert-Bucy[ Ether (ETBE) 57 07 50 000000 0 114 1 64-138 <br /> tert Amyl Methyl Ether I I 53 84 I I 1� 50 000000 0 91 105 9 € 67-154 <br /> I <br /> IE I I ! 1 I' Page 13 * =Y. REG, R=RPD, A=ABS Diff D=% Diff I <br /> I <br /> it I i <br /> ' II <br /> � I I Ir I I E I 11!11 Ills I I <br /> �I I{ II II III (i a II II 11 II II kl " I I III 11 Illy AI <br />