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Q UAL I T Y C O N T R O L R E 5 U L T S <br /> Job Number 992709 Report Date 01/06/2000 <br /> CUSTOMER 1T Group PROJECT Southland - Martinez ATTN Rhonda Telcheira <br /> QC Type Description Reig Code Lab ID Dilution Factor Date Time <br /> MS Matrix Spike 09120705 992636-2 12/24/1999 0225 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> ethyl-t-Butyl Ether (MTBE) _ 141 59 100 000000 20 29 121 3 71-142 <br /> 1,2 pichloroethane 10 26 10 000000 0 102 6 70-130 <br /> 1,2-Dibromoethane (EDB) 10 77 10 000000 0 107 7 70-130 <br /> MSD Matrix Spike Duplicate 09120705 992636-2 12/24/1999 0259 <br /> Parameter/Test Description QC Result QC Result True Value Ori, Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 982.02 1161 58 1000 000000 1 80 98 0 34-182 <br /> 17 19 <br /> Di-Isopropyl Ether 55 30 61 54 50 000000 0 110 6 60-131 <br /> 11 24 <br /> thyl tert-Butyl Ether (ETBE) 52.73 57 07 50 000000 0 105 5 64-138 <br /> t <br /> 8 29 <br /> tert-Amyl Methyl Ether 51 98 53 84 50 000000 0 91 102 1 67-154 <br /> 4 27 <br /> Ip <br /> 4l-t-Butyl Ether (MTBE) 121 56 141 59 100 000000 20 29 101 3 71-142 <br /> 15 31 <br /> 1,Z Dichloroethane 9 90 10 26 10 000000 0 90 70-130 <br /> 4 30 <br /> 1,2-Dibromoethane (EDB) 9 18 10 77 10 000000 0 91 8 70-130 <br /> 1 16 30 <br /> LCS Laboratory Control Sample 09123101 01/04/2000 0636 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 1090 83 1000 000000 109 1 37-1,75 <br /> D1-Isopropyl Ether 48 73 50 000000 97 5 60-138 <br /> Ethyl tert-Butyl Ether (ETBE) 52 59 50 000000 105 2 51-143 <br /> tert-AmyL Methyl Ether 49 15 50 000000 98 3 64-137 <br /> MethyL-t-Butyl Ether (MTBE) 97 57 100 000000 97 6 33-169 <br /> 9 96 10 000000 99 6 70-130 <br /> ,1,1-0,clloroethane <br /> 1,2-Dibromoethane (EDB) 9 92 10 000000 99 2 70-130 <br /> Mf8 Method Blank <br /> I 4' 01/04/2000E42] <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 0 <br /> D1-Isopropyl Ether 0 <br /> Ethyl tert-ButyL Ether (ETBE) 0 <br /> tert-Amyl MethyL Ether 0 <br /> Methyl-t-Butyl Ether (MTBE) 0 <br /> 1,2-Dichloroethane 0 <br /> 2-Dibromoethane (EDB) 0 <br /> ' I <br /> 6 1 h I I Page 14 * Y=X REG, R=RPD, A=ABS Diff D=% Diff, <br /> , <br />