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CALIFORNIA LABORATORY SERVICES <br /> Page 8 of 12 12/29/08 13:12 <br /> E2C Remediation Project: Busy Bee Lodi <br /> 1358 Blue Oaks Drive, Suite 300 Project Number: [none] CLS Work Order#:CRL0743 <br /> Roseville.CA 95678 Project Manager: Greg Brandin COC#:96210 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %RLC Limits RPD Limit Notes <br /> Batch CR10555- EPA 5030 Water MS <br /> Matrix Spike(CR10555-MSI) Source:CRL0743-01 Prepared&Analyzed: 12/22/08 <br /> Trichloroethene 23.4 0.50 Ng/L 20.0 2.15 106 55-138 <br /> Surrogate: 1,2-Dichloroethane-d4 9.16 10.0 93 66-135 <br /> Surrogate:Toluene-d8 10.7 10.0 107 72-115 <br /> Surrogate:4-Bromofluorobenzene 9.55 10.0 96 73-125 <br /> Matrix Spike Dup(CR10555-MSD_1) Source:CRL0743-01 Prepared: 12/22/08 Analyzed: 12/23/08 <br /> Benzene 21.9 0.50 pg/L 20.0 ND 110 52-139 0.9 25 <br /> Chlorobenzene 22.2 0.50 20.0 ND Ill 62-134 3 25 <br /> I,1-Dichloroethene 29.6 0.50 20.0 1.35 141 32-152 0.07 25 <br /> Toluene 23.0 0.50 20.0 ND 115 58-139 3 25 <br /> Trichloroethene 22.7 0.50 20.0 2.15 103 55-138 3 25 <br /> Surrogate: 1,2-Dichloroethane-d4 9.36 10.0 94 66-135 <br /> Surrogate:Toluene-d8 10.7 10.0 107 72-125 <br /> Surrogate:4-BromoJluorobenzene 9.51 10.0 95 73-125 <br /> Batch CR10601 - EPA 5030 Water MS <br /> Blank(CR10601-BLKI) Prepared&Analyzed: 12/23/08 <br /> Acetone ND 10 µg/L <br /> Benzene ND 0.50 " <br /> Bromobenzene ND 0.50 " <br /> Bromochloromethane ND 0.50 " <br /> Bromodichloromethane ND 0.50 " <br /> Bromoform ND 0.50 " <br /> Bromomethane ND 1.0 " <br /> 2-Butanone ND 10 " <br /> n-Butylbenzene ND 0.50 " <br /> sec-Butyl benzene ND 0.50 " <br /> tert-Buty I benzene ND 0.50 " <br /> Carbon tetrachloride ND 0.50 " <br /> Chlorobenzene ND 0.50 " <br /> Chloroethane ND 0.50 " <br /> CA DOHS FLAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.californialab.com 916-638-7301 Fax: 916-638-4510 <br />