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CALIFORNIA LABORATORY SERVICES <br /> Page 10 of 12 12/29/08 13:12 <br /> E2C Remediation Project: Busy Bee Lodi <br /> 1358 Blue Oaks Drive, Suite 300 Project Number: [none] CLS Work Order#:CRL0743 <br /> Roseville,CA 95678 Project Manager: Greg Brandin COC#:96210 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Reporting Spike Source %REC RPD <br /> kmlk tc Result Limit Units Level , Result %REC Limits RPD Limit Notes <br /> Batch CR10601 - EPA 5030 'Vater MS <br /> Blank(CR10601-BLKI) Prepared&Analyzed: 1223/08 <br /> 4-Methyl-2-pentanone ND 10 pg/L <br /> Methyl tert-butyl ether ND 0.50 " <br /> Naphthalene ND 0.50 " <br /> n-Propylbenzene ND 0.50 " <br /> Styrene ND 0.50 " <br /> 1,1,1,2-Tetrachloroethane ND 0.50 " <br /> 1,1,2,2-Tetrachloroethane ND 0.50 " <br /> Tetrachloroethene ND 0.50 " <br /> Toluene ND 0.50 " <br /> 1,2,3-Trichlorobenzene ND 0.50 <br /> 1.2,4-Trichlorobenzene ND 0.50 " <br /> 1,1,1-Trichloroethane ND 0.50 " <br /> 1,1,2-Trichloroethane ND 0.50 " <br /> Trichloroethene ND 0.50 " <br /> Trichlorofluoromethane ND 0.50 " <br /> 1,2,3-Trichloropropane ND 0.50 " <br /> 1,2,4-Trimethylbenzene ND 0.50 <br /> 1,3,5-Trimethylbenzene ND 0.50 " <br /> Vinyl chloride ND 1.0 " <br /> Xylenes(total) ND 1.0 " <br /> Surrogate: 1,2-Dichloroethane-d4 9.93 10.0 99 66-135 <br /> Surrogate:Toluene-d8 10.5 10.0 105 72-125 <br /> Surrogate:4-Bromofluorobenzene 10.1 10.0 101 73-125 <br /> LCS(CR10601-BSI) --Prepared&Analyzed: 12/23/08 <br /> Benzene 21.9 0.50 pg/L 20.0 110 60-135 <br /> Chlorobenzene 22.0 0.50 20.0 110 60-133 <br /> 1,1-Dichloroethene 23.8 0.50 20.0 119 42-150 <br /> Toluene 23.0 0.50 20.0 115 60-137 <br /> Trichloroethene 22.0 0.50 20.0 110 62-140 <br /> Surrogate. 1,2-Dichloroethane-d4 10.2 10.0 .102 66-135 <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.californialab.com 916-638-7301 Fax: 916-638-4510 <br />