APEX E,NVIROTECH, INC.
<br /> STANDARDbPERAMNG PROCEDURE
<br /> Mon tonna lNells
<br /> SOP - 4
<br /> SOP " 7 p'? SAMPLE IDENTIFICATION AND CHA_ IIN-
<br /> SOfL BORING SAMPLING = OF-CUSTODY PROCEDURES
<br /> During drilling,.soil samples for chemical analysis are collected Sample identification and chain-of-custody procedures ensure
<br /> in thin-walled brass tubes,of varying diameters and lengths sample integrity as well as.document sample possession from
<br /> (e.g.,4 or 6 inches long by 2 inches outside diameter). Three the time of collection to ultimate disposal. Each sample
<br /> or four of the selected tubes,plus a spacer tube,are set in an container submitted for analysis is labeled to identify the job
<br />_ 184nch long split-barrel sampler of the appropriate inside- number,date,time of sample collection,a sample number
<br /> diameter. unique to the sample,any in-field measurements made,
<br /> sampling methodology,name(s)of on-site personnel,and any
<br /> Where possible;'I!pe split-barrel sampler is driven its entire other pertinent field observations also recorded on the field
<br /> length ether hydraulically or using a 140-pound drop hammer. excavation or boring log.
<br /> The sampler is kracted from the borehole and the brass
<br /> tubes,containing the soil samples,are removed. Upon removal Chain-of-custody forms are used to record possession of.the
<br /> from the sampler,the selected brass tubes are either sample from time of collection to arrival at the iaborator}.
<br /> immediately trimmed and capped with aluminum foil or"Teflon" During shipment,the person with custody of the samples will
<br /> sheets and plastic caps or the samples are extruded from the relinquish them to the next person by signing the.chain-of-
<br /> tubes and sealed within other appropriate,cleaned sample custody form(s)and noting the date and time. The sample-
<br /> containers. The samples are then hermetically sealed,labeled, control officer at the laboratory will verify sample integrity, .
<br /> and refrigerated For delivery,under strict chain-of-custody,to correct preservation,confirm collection in the proper
<br /> the analytical laboratory. These procedures minimize the corrtainer s ,and ensure ad }
<br /> r, ( ) equate volume for analysis.
<br /> potential for cross-contamination and volatilization of volatile
<br /> organic compounds(VOC)prior to chemical analysis. If these conditions are met,the samples will be assigned
<br /> unique laboratory log numbers for identification throughout
<br /> One soil sample collected at each sampling interval is analyzed analysis and reporting. The log numbers will be recorded on
<br /> 4.
<br /> in the field using;lether a portable photoionization detector the chain-of-custody farms and in the legally-required log book
<br /> (PID),flame ioni�m ion detector,organic vapor analyzer, maintained in the laboratory. The sample description,date
<br /> catalytic gas detector,or an ex plosimeter. The purpose of this received,client's name,and any other relevant information will s,f?
<br /> field analysis is to'qualitatively determine the presence or also be recorded.
<br /> absence of hydrocarbons,and the samples to be analyzed at
<br /> the laboratory. The soil sample is sealed in either a brass tube,
<br /> glass jar,or plastic bag to allow for some volatilization of VOC. SOP - 5
<br /> The PfD is then used to measure the concentrations of. LABORATORY ANALYTICAL QUALITY
<br /> hydrocarbons within the containers's headspace. The data isASSURANCE AND CONTROL
<br /> recorded on both field notes and the boring logs at the depth J.
<br /> corresponding.to•the sampling point. In addition to routine instrument calibration,replicates,spikes,
<br /> blanks,spiked blanks,and certified reference materials are
<br /> Other soil samples are collected to document the soil and/or routinely analyzed at method-specific frequencies to monitor
<br /> stratigraphic profile beneath the project site;and estimate the precision and bias. Additional components of the laboratory-
<br /> relative permeability of the subsurface materiels. All drilling Quality Assurance/Quality Control program include:
<br /> and sampling equipment are either steam cleaned or washed in ,
<br /> solution and doubly rinsed in dsionized water prior to use at 1, Participation in state and federal laboratory
<br /> each site and between boreholes to minimize the potential for accreditation/certification programs;
<br /> cross-contamination.
<br /> 2. Participation in both U.S. EPA Performance
<br /> In the evert the soil samples cannot be submitted to the Evaluation studies(WS and WP studies)and inter-
<br /> analytical laboratory on the same day they are collected(e.g., laboratory performance evaluation programs;
<br /> due to weekends'or holidays),the samples are temporarily
<br /> stored until the first opportunity for submittal either oh ice in a S• Standard operating procedures describing routine
<br /> cooler,such as when in the field,or in a refrigerator at Apexes and periodic instrument maintenance;
<br /> office.
<br /> 4.. "Out-of-ControP/Corrective Action documentation
<br /> SOP - 3 procedures;and,
<br /> SOIL CLASSIFICATION 5.. Multi-level review of raw data and client reports.
<br /> Soil samples are classified according to the Unified Soil
<br /> Classification System. Representative portions of the samples SOP - g
<br /> may be submitted,under strict chain-cf-custody,to an HOLLOW-STEM AUGER MONITORING'
<br /> analytical laboratory for further examination and verification of WELL INSTALLATION AND
<br /> the in-field classification and analysis of soil mechanical and/or DEVELOPMENT
<br /> petrophysical properties. The soil types are indicated on logs
<br /> of either excavations or borings together with depths Boreholes for monitoring wells are drilled using a truck-
<br /> corresponding to the sampling paints and other pertinent mounted,hollow-stem auger drill rig. The borehole diameter
<br /> information, will be a minimum of 4 inches larger than the outside diameter
<br /> of the casing when installing well screen. The hollow-stem
<br /> auger provides minimal interruption of drilling while permitting
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