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ANALYTICAL <br /> BS-IkLABORATORIES <br /> • Ery Rifenburg Certificate of Analysis <br /> Foothill Engineering ELAP Certificate #1180 <br /> 1.2793 Paddy Creek Lane Report Issue Date 06/12/2003 <br /> Lodi, CA 95240 <br /> BSK Submission#: 2003051843 <br /> BSK Sample ID# 327124 <br /> Project ID Project Desc Connell Motor Truck <br /> Submission Comments <br /> Sample Type Solid Date Sampled 05/27/2003 <br /> Sample Description MW1D at 60 Time Sampled 1300 <br /> Sample Comments Date Received 05/29/2003 <br /> Organics <br /> prep Analysts <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 1600 mg/Kg 1 50 50 06/04/03 06/05/03 <br /> Benzene EPA 8020 35 mg/Kg 0 005 50 0254 06/04/03 06/05/03 <br /> Ethylbenzene EPA 8020 80 mg/Kg 0 005 50 0 250 06/04/03 06/05/03 <br /> Toluene EPA 8020 83 mg/Kg 0 005 50 0 250 06/04/03 06/05/03 <br /> Total Xylenes EPA 8020 120 mg/Kg 0 005 500 2 500 06/05/03 06/05/03 <br /> 1,2-Dibromoethane EPA 8260 ND gg/Kg 50 50 250 06/07/03 06/07/03 <br /> 1,2-Dichloroethane EPA 8260 ND pg/Kg 50 50 250 06/07/03 06/07/03 <br /> Di-isopropyl Ether EPA 8260 ND lig/Kg 50 50 250 06/07/03 06/07/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND pg/Kg 50 50 250 06/07/03 06/07/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND pg/Kg 50 50 250 06/07/03 06/07/03 <br /> t-Amyl Methyl Ether EPA 8260 ND pg/Kg 50 50 250 06/07/03 06/07/03 <br /> tert-Butyl Alcohol EPA 8260 ND gg/Kg 50 50 2500 06/07/03 06/07/03 <br /> Surrogate <br /> -- - - -- ---- --- - - - ----- - -- - <br /> Fluorobenzene EPA 8020 9633 %Rec - 50 N/A 06/04/03 06/05/03 <br /> Toluene-0 EPA 8260 74 %Rec 50 N/A 06/07/03 06/07/03 <br /> mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> pg/L Micrograms/Liter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> gg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report Authentication Code IHIM Hill 111111 101Hill[191191111111111111111Hill Hill 111111KIIIII Page 2 of 20 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />