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5 ANALYTICAL <br /> BSKLABORATORIES <br /> • Ery Rifenburg Certificate of Analysis <br /> Foothill Engineering ELAP Certificate #1180 <br /> 12793 Paddy Creek Lane Report issue Date 06/12/2003 <br /> Lodi, CA 95240 <br /> BSK Submission#: 2003051843 <br /> BSK Sample ID#, 327125 <br /> Project 1D Project Desc Connell Motor Truck <br /> Submission Comments <br /> Sample Type Solid Date Sampled 05/27/2003 <br /> Sample Description MW1D at 65 Time Sampled 1300 <br /> Sample Comments Date Received 05/29/2003 <br /> Organics prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 53 mg/Kg 1 1 1 06/04/03 06/04/03 <br /> Benzene EPA 8020 0 042 mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Ethylbenzene EPA 8020 0 016 mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Toluene EPA 8020 0 011 mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Total Xylenes EPA 8020 0 069 mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> 1,2-Dibromoethane EPA 8260 ND jig/Kg 50 1 5 06/07/03 06/07/03 <br /> 1,2-Dichloroethane EPA 8260 55 gg/Kg 50 1 so 06/07/03 06/07/03 <br /> Di-isopropyl Ether EPA 8260 ND µg/Kg 50 1 5 06/07/03 06/07/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND µg/Kg 50 1 5 06/07/03 06/07/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND µg/Kg 50 1 5 06/07/03 06/07/03 <br /> t-Amyl Methyl Ether EPA 8260 ND µg/Kg 50 1 5 06/07/03 06/07/03 <br /> tert-Butyl Alcohol EPA 8260 ND 4g(Kg 50 1 50 06/07/03 06/07/03 <br /> Surrogate <br /> - - - - -- - - -- --- - - - - -- ---- --- - - -- - -- - - - -- - --- - -- - - -- -- - -- - - -- - - - - - - - - <br /> Fluorobenzene EPA 8020 852 %Rec - I N/A 06/04/03 06/04/03 <br /> Toluene-d8 EPA 8260 100 %Rec I N/A 06/07/03 06/07/03 <br /> 49 mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> pg/L Micrograms/Liter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> gg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report Authentication Code 11111111 Hill 1911 HIM Hill Hill 1111111111 Hill[all U1 1111111111111111111101 IN 11111 Page 3 of 20 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />