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' 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> Mccampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.nic6anipbell.com E-mail:main campbell.com <br /> Advanced GeoEnvironmental,Inc. Client Project ID: Connell Motor Truck Date Sampled: 07/09/03 <br /> ' • 837 Shaw Road Sales Date Received: 07/11/03 <br /> ' Client Contact: Bill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> Volatiles Organics+Oxygenates by P&T and GUMS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0307177 <br /> Lab ID 0307177-004B ___ <br /> ' Client ID MW4 <br /> Matrix Water <br /> Reporting <br /> Compound Concentration* DF Re <br /> DF orting Compound Concentration* DF Limit <br /> ' Acetone --- - - ND 1.0 5.0 tert-Am 1 methyl ether(TAME) ND 1.0 0.5 <br /> Benzene ND 1.0 0.5 Bromobenzene ND 1.0 0.5 <br /> Bromochloromethane _ ND 1.0 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform ND 1.0 0.5 Bromomethane ND 1.0 0.5 <br /> 2-Butanone EK ND 1.0 1.0 t-Butyl alcohol A) ND 1.0 5.0 <br /> ' <br /> n-Butyl benzene ND 1.0 0.5 sec-Butyl benzene ND 1.0 0.5 <br /> tert-Butyl benzene ND 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene ND 1.0 0.5 <br /> Chloroethane ND 1.0 0.5 2-Chloroeth 1 Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane ND 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlorotoluene ND 1.0 0.5 <br /> Dibromochloromethane ND 1.0 0.5 1,2-Dibromo-3-chloro ro ane ND 1.0 0.5 <br /> 1,2-Dibromoethane DB) ND 1.0 0.5 Dibromomethane ND 1.0 0.5 <br /> 1,2-Dichlorobenzene ND 1.0 0.5 1,3-Dichlorobenzene ND 1.0 0.5 <br /> 1,4-Dichlorobenzene ND 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> • 1,1-Dichloroethane ND 1.0 0.5 1,2-Dichloroethane(1,2-DCA ND 1.0 0.5 <br /> l1,1-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-l,2-Dichloroethene ND 1.0 0.5 1,2-Dichloro ro ane ND 1.0 0.5 <br /> 1,3-Dichloro ro ane ND 1.0 0.5 2,2-Dichlororo ane ND 1.0 0.5 <br /> ' 1,1-Dichloropro ene ND 1.0 0.5 cis-1,3-Dichlororo ene ND 1.0 0.5 <br /> trans-1,3-Dichloro ro ene ND 1.0 0.5 Diiso ro yl ether IPE ND 1.0 0.5 <br /> Eth lbenzene ND 1.0 0.5 Ethyl tert-butyl ether(ETBE) ND 1.0 0.5 <br /> Hexachlorobutadiene ND 1.0 0.5 2-Hexanone ND 1.0 0.5 <br /> ' Iodomethane(Methyl iodide ND 1.0 5.0 Isopropylbenzene ND 1.0 0.5 <br /> 4-1sopropyl toluene ND 1.0 0.5 Meth 1-t-bu 1 ether MTBE ND 1.0 0.5 <br /> Methylene chloride ND 1.0 0.5 4-Meth 1-2- entanone I3K) ND 1.0 0.5 <br /> Naphthalene ND 1.0 0.5 -n-Propyl benzene ND 1.0 0.5 <br /> Styrene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1.0 0.5 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND 1.0 0.5 <br /> Toluene ND 1.0 0.5 1,2,3-Trichlorobenzene ND 1.0 0.5 <br /> 1,2,4-Trichlorobenzene ND 1.0 0.5 1,1,1-Trichloroethane ND 1.0 0.5 <br /> ' 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichloro ro ane ND 1.0 0.5 <br /> 1,2,4-Trimeth lbenzene ND 1.0 0.5 1,3,5-Trimethlbenzene ND 1.0 0.5 <br /> Vinyl Acetate ND 1.0 5.0 Vin l'Chloride ND 1.0 1 0.5 <br /> ' Xylenes ND 1.0 1 0.5 <br /> Surrogate Recoveries(%) <br /> %SS 1: 103 %SS2: 100 <br /> ' %SS3: 110 <br /> Comments: <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oiVnon-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> or anic content. <br /> ' DHS Certification No. 1644 Angela Rydehus,Lab Manager <br />