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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> [4 <br /> MCCampbell Analytical hlc. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccanipbell.com E-mail:nlain@rwcampbefl.com <br /> ' Advanced GeoEnvironmental,Inc. Client Project ID: Connell Motor Truck Date Sampled: 07/09/03 <br /> • 837 Shaw Road Sales Date Received: 07/11/03 <br /> ' Client Contact: Bill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS-(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0307177 <br /> Lab ID 0307177-005B <br /> ' Client ID MW5 <br /> - - Matrix Water <br /> Reporting <br /> Compound Concentration* DF S g Compound Concentration* DF Un* <br /> ' Acetone ND 1.0 5.0 tert-Am I methyl ether(TAME) ND 1.0 1 0.5 <br /> Benzene ND 1.0 0.5 Bromobenzene ND 1.0 0.5 <br /> Bromochloromethane ND 1.0 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform _ ND 1.0 0.5 Bromomethane ND 1.0 0.5 <br /> ' 2-Butanone(MEK) ND 1.0 1.0 t-Butyl alcohol(TBA) ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 0.5 sec-Butyl benzene 1.3 1.0 0.5 <br /> tert-Butyl benzene ND 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene 1.1 1.0 0.5 <br /> ' Chloroethane ND 1.0 0.5 2-Chloroeth I Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane ND 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlorotoluene ND 1.0 0.5 <br /> Dibromochloromethane ND 1.0 0.5 1,2-Dibromo-3-chloro ro ane ND 1.0 0.5 <br /> 1,2-Dibromoethane(EDB) ND 1.0 0.5 Dibromomethane ND 1.0 0.5 <br /> 1,2 Dichlorobenzene 9.7 1.0 0.5 1,3-Dichlorobenzene ND 1.0 0.5 <br /> 1,4-Dichlorobenzene ND 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> ' . 1,1-Dichloroethane ND 1.0 0. 1,2-Dichloroethane 1,2-DCA 27 1.0 0.5 <br /> 1,1-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-1,2-Dichloroethene ND 1.0 0.5 1,2-Dichlororo ane 1.2 1.0 0.5 <br /> 1,3-Dichloro roane ND 1.0 0.5 2,2-Dichlororo ane ND 1.0 0.5 <br /> ' 1,1-Dichlororoene ND 1.0 0.5 cis-1,3-Dichloroo ene ND 1.0 0.5 <br /> trans-l,3-Dichloro rone ND 1.0 0.5 Diiso ro 1 ether IPE) ND 1.0 0.5 . <br /> Ethylbenzene ND 1.00.5 Ethyl tert-butyl ether ETBE ND 1.0 0.5 <br /> Hexachlorobutadiene ND 1.0 0.5 2-Hexanone ND 1.0 0.5 <br /> ' Iodomethane(Methyl iodide ND 1.0 5.0 Isom lbenzene 1.2 1.0 0.5 <br /> 4-Isopropyl toluene ND 1.0 0.5 Meth l-t-bu l ether TBE ND 1.0 0.5 <br /> Methylene chloride ND 1.0 0.5 4-Methyl-2- entanone MIBK ND 1.0 0.5 <br /> Naphthalene ND 1.0 0.5 n-Prol benzene 1.5 1.0 0.5 <br /> ' <br /> Styrene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1.0 0.5 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND 1.0 0.5- <br /> Toluene ND 1.0 0.5 1,2,3-Trichlorobenzene ND 1.0 0.5 <br /> 1,2,4-Trichlorobenzene ND 1.0 0.5 1,1,1-Trichloroethane ND 1.0 0.5 <br /> ' 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichloro ro ane ND 1.0 0.5 <br /> 1,2,4-Trimeth lbenzene 1.5 1.0 0.5 1,3,5-Trimeth (benzene 5.1 1.0 0.5 <br /> Vinyl Acetate ND 1.0 5.0 Vinyl Chloride ND 1.0 0.5 <br /> ' Xylenes ND 1.0 0.5 <br /> Surrogate Recoveries(%) <br /> %SSI: 7 103 %SS2: 98.8 _ <br /> ' %SS3: 105 <br /> Comments:i <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> •#surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> or anic content. <br /> ' DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />