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B. If a new purge volume is selected after additional step purge tests <br /> are conducted, the soil gas investigation should be continued as <br /> follows: <br /> 1. In areas of the same or similar lithologic conditions: <br /> a. Re-sample 20 percent of the previously completed probes. <br /> This re-sampling requirement may be reduced or waived in <br /> consultation with Agency staff, depending on site <br /> conditions. If re-sampling indicates higher detections (e.g., <br /> more than 50 percent difference in samples detected at <br /> greater than or equal to 10µg/L), all other previous probes <br /> should be re-sampled using the new purge volume. <br /> b. Continue the soil gas investigation with the newly selected <br /> purge volume in the remaining areas. <br /> 2. In areas of different lithologic conditions: Continue the soil gas <br /> investigation with the newly selected purge volume in the <br /> remaining areas. <br /> 2.4 Leak Test <br /> Leakage during soil gas sampling may dilute samples with ambient air and <br /> produce results that underestimate actual site concentrations or contaminate <br /> the sample with external contaminants. Leak tests should be conducted to <br /> determine whether leakage is present(e.g.,the leak check compound is <br /> detected and confirmed in the test sample after its application). <br /> 2.4.1 Leak tests should be conducted at every soil gas probe. <br /> 2.4.2 Leak Check Compounds: Tracer compounds, such as pentane, <br /> isopropanol, isobutene, propane, and butane, may be used as leak <br /> check compounds, if a detection limit (DL) of 10 µg/L or less can be <br /> achieved. These compounds may be contained in common products <br /> such as shaving cream. <br /> 2.4.3 A leak check compound should be placed at any location where <br /> ambient air could enter the sampling system or where cross <br /> contamination may occur, immediately before sampling. Locations of <br /> potential ambient air intrusion include: <br /> A Sample system connections; <br /> B. Surface bentonite seals(e.g., around rods and tubing); or <br /> C. Top of the Temporary Soil Gas Probe (see Section 2.2.5.13). <br /> 01/28/2003 - 10- <br />