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DHS ELAP Certification No 1644 IIVV- Angela Rydelius, Lab Manager ✓ McCa ipbell Analytical, Inc. ' "When Ouslit,C t" I 34 CA : ,,mcca PassRoad,Finail: ain@m 65-1701 Web: www.mccamphell.com E-mail: mvnQmccempbell.wm Tcleohone: 877-252-9262 Fax: 925-252-9269 ' Ponder Environmental Services 220 East G Street Benicia, CA 94510 Client Project ID: Tank 3302 Date Sampled: 01/29/08 Date Received: 01/29/08 Client Contact: Jim Ponder Date Extracted: 02/05/08-02/06/08 Client P.O.: Date Analyzed 02/11/08 Volatile Organics by GUMS (Basic Target List)* Extraction Method: SW13lllZHETCLP)/SW50308 Analytical Method: SW8260B Work Order. 0801699 Lab ID 0801699-OOIA Client ID 1701-1 Matrix Solid Compound Concentration* DF aLns Compound Concentration* DF as Acetone 2200 1000 0.2 Acrolein Pro en ND<5.0 1000 0,005 Actylonittile <2.0 No0 0.002 tert-Am 1 meth 1 ether TAME ND<0.50 1000 0.0005 Benzene 1 0.64 1 0 0.0005 Bromobenzene ND<0.50 1000 0.0005 Bromochloromethane <0.50 1 00 0.0005 Brom dichloromethane ND<0.50 1000 0.0005 Bromoform N <0.50 000 0.0005 Bromomethane ND<0.50 1000 0.0005 2-Butamme MEK) ND 0 1000 0.5 t-But 1 alcohol TBA ND<50 1000 0 05 n-Butyl benzene ND<0.50 1000 0.0005 sec-Butyl benzene ND<0.50 1000 0.0005 tert-Butyl benzene ND<0.50 1000 0,0005 Carbon Disulfide ND<0.50 1000 0.0005 Carbon Tetrachloride ND<0.50 1000 0.0005 Chlorobenzene ND<0.50 1000 0.0005 Chloroethane ND<0.50 1 1000 0.0005 2-Chloroeth 1 Vinyl Ether ND<I.0 1000 10.001 Chloroform ND<0.50 00 0.0005 1 Chloromethane ND<0.50 1000 10.0005 2-Chlorotoluene ND<0.50 1000 0.0005 4-Chlorotoluene ND<0.50 1000 0.0005 Dibromochloromethane ND<0.50 lQ00 0.0005 1 2-Dibr mo-3-chloro ro ane N < . 0 1000 0.0005 ] 2-Dibromoethane EDB ND<0.50 1000 0.0005 Dibromometh ne ND<0.50 1000 0.0005 1,2-Dichlorobenzene ND<0.50 1000 0.0005 1.3-Dichlorobenzene ND< . 0 1000 0.0005 1 .4-Dichlorobenzene ND<0.50 1000 0,0005 Dichl ro iflu romethane ND<0.50 0 0.00 5 11-Dichloroethane ND<0.50 1000 0.0005 12-Dichloroethane 12-DCA ND<0.50 1000 0.0005 l 1-Dichloroethene ND<0.50 1000 0.0005 cis- 12-Dichl roethene ND<0.50 1000 0.0005 trans-1 2-Dichloroethene ND<0.50 1000 0.0005 1 2-Dichl rc ro ane ND<0.50 1000 0.0005 1 3- ichl ro ro ane ND<0.50 1000 10,0005 2 2-Dichlor ro ane ND<0.50 1 0.0005 1 1-Dichlor ro ene ND<0.50 1000 0.0005 cis-1 3-Dichl ro ro ene ND<0.50 1000 0.0005 trans- I3-Dichlor ro ene ND<0.50 1000 0,0005 Diisopropyl ether DIPS ND<0.50 1000 0,0005 Eth (benzene 4.5 1000 0.0005 Ethyl ten-butyl ether ETBE ND<0.50 3000 0.0005 Freon 113 ND<IO 1000 0.01 Hexachlorobutadiene ND<0.50 1000 0.0005 Hexachl roethane ND<0.50 1000 0.0005 2-He an ne NDQO 1000 0.02 Iso ro lbenzene ND<0.50 1000 0.0005 4-Isopropyl toluene ND<0.50 1000 0.0005 Met 1-t- ut 1 ether TBE ND<0.50 1000 0.0005 Methylene chloride <5.0 1000 0,005 4-Meth 1-2- entanone IBK ND<5.0 1000 0.005 Naphthalene 0.93 1000 0.0005 Nitrobenzene ND<10 1000 0.01 I n-Pro vl benzene 0.70 1000 0.0005 rvrene ND<0.50 1000 00005 1112-Tetrachloroethan <050 1000 0.0005 1,1 22-Tetrachloroethane ND<0.50 1000 0.0005 Tetrachloroethene ND<5 0 1000 0.005 Toluene 14 1000 0.005 1 2 3- richt r ben ene ND<0.50 1000 0.0005 1 24-Trichl r- enzene - --FD<0.50-- --1000-- 0 0005 1.1.1-Trichloroethane ND<0.50 1000 0.0005 112-Trichloroethane ND<0.50 1000 0.0005 Trichloroethene ND<5.0 1000 0.005 Trichl r flu r methane <0.50 1000 0.000 2 3-Trichlororo ane ND<0.50 1000 0:0005 124-Trimeth ]benzene 7.1 1000 0.0 05 135-Trimeth (benzene 1.8 1000 0.0005 < 5 5 ec Surrogate Roveries %SSI: 111 % S2: 99 Comments: * water and vapor samples are reported in pg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are reported in mg/L, wipe samples in gg/wipe. ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis. surrogate diluted out of range or surrogate coe utes with another pea low/high surrogate recovery due to matrix mer erence. h) lighter than water immiscible sheen/product is present; i) liquid sample that contains greater than -1 vol. % sediment; j) sample diluted due to high organic content/matrix interference; k) reporting limit near, but not identical to our standard reporting limit due to variable Encore sample weight; m) reporting limit raised due to insufficient sample amount; n) results are reported on a dry weight basis; ) see attached narrative. DHS ELAP Certification No 1644 IIVV- Angela Rydelius, Lab Manager