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COMPLIANCE INFO_PRE 2019
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COMPLIANCE INFO_PRE 2019
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Last modified
1/7/2020 10:49:01 AM
Creation date
1/7/2020 9:49:15 AM
Metadata
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Template:
EHD - Public
ProgramCode
2200 - Hazardous Waste Program
File Section
COMPLIANCE INFO
FileName_PostFix
PRE 2019
RECORD_ID
PR0513950
PE
2247
FACILITY_ID
FA0009657
FACILITY_NAME
NUSTAR TERMINALS OPERATIONS PARTNERSHIP LP
STREET_NUMBER
2941
STREET_NAME
NAVY
STREET_TYPE
DR
City
STOCKTON
Zip
95206-1149
APN
48906-1
CURRENT_STATUS
01
SITE_LOCATION
2941 NAVY DR
P_LOCATION
01
P_DISTRICT
001
QC Status
Approved
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MCCampbell Analytical, Inc. 536 Willow Road PE-inaig,CA 945�6oc5�7P1 <br />Web: www bell.com Email: main be8.com <br />'-When Quality Counts" Telephone: 877-252-9262 Fax: 925-252-9269 <br />QC SUMMARY REPORT FOR SW8270D <br />W.O. Sample Matrix: Soil QC Matra: Soil WorkOrder: 0801699 <br />EPA Method: SW8270D <br />Extraction: SW1311/SW3510C <br />BatchlD: 33632 <br />Spiked Sample ID: <br />N/A <br />Analyte <br />Sample <br />mg/L <br />Spiked <br />mg/L <br />MS <br />% Rea <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rea <br />LCSD <br />% Rec. <br />LCS-LCSD Acceptance Criteria <br />% RPD MS / MSD RPD LCS/LCSD <br />RPD <br />Acenaphthene <br />N/A <br />0.050 <br />N/A <br />N/A <br />N/A <br />98.7 <br />98.6 <br />0.142 <br />N/A <br />N/A <br />1 30- 130 <br />30 <br />4-Chloro-3-methylphenol <br />N/A <br />0.10 <br />N/A <br />N/A <br />N/A <br />107 <br />103 <br />4.02 <br />N/A <br />N/A <br />30-130 <br />30 <br />2 -Chlorophenol <br />N/A <br />0.10 <br />N/A <br />N/A <br />N/A <br />107 <br />106 <br />0.957 <br />N/A <br />N/A <br />30-130 <br />30 <br />1,4 -Dichlorobenzene <br />N/A <br />0.050 <br />N/A <br />N/A <br />N/A <br />63.2 <br />63.5 <br />0.379 <br />N/A <br />N/A <br />30-130 <br />30 <br />2,4-Dinitrotoluene <br />N/A <br />0.050 <br />N/A <br />N/A <br />N/A <br />111 <br />110 <br />0.571 <br />N/A <br />N/A <br />30-130 <br />30 <br />4-Nitrophenol <br />N/A <br />N/A <br />N/A <br />75.4 <br />76.7 <br />1.78 <br />N/A <br />N/A <br />30-130 <br />30 <br />N-Nitrosodi-n-propylatnine <br />N/A <br />N/A <br />N/A <br />101 <br />99.6 <br />1.15 <br />N/A <br />N/A <br />30-130 <br />30 <br />Pentachlorophenol <br />N/A <br />N/A <br />N/A <br />93.5 <br />91.7 <br />2.02 <br />N/A <br />N/A <br />30-130 <br />30 <br />Phenol <br />tN/A5 <br />N/A <br />N/A <br />N/A <br />85.7 <br />86.4 <br />0.854 <br />N/A <br />N/A <br />30-130 <br />30 <br />Pyrene <br />N/A <br />N/A <br />N/A <br />119 <br />118 <br />0.558 <br />N/A <br />N/A <br />30-130 <br />30 <br />1,2,4-Trichlorobenzene <br />N/A <br />N/A <br />N/A <br />79.1 <br />78.1 <br />1.30 <br />N/A <br />N/A <br />30-130 <br />30 <br />%SSI: <br />N/A <br />N/A <br />N/A <br />98 <br />88 <br />0 <br />N/A <br />N/A <br />30-130 <br />30 <br />%SS2: <br />N/A <br />N/A <br />N/A <br />82 <br />82 <br />0 <br />N/A <br />N/A <br />30-130 <br />30 <br />%SS3: <br />N/A <br />5 <br />N/A <br />N/A <br />N/A <br />105 <br />104 <br />1.15 <br />N/A <br />N/A <br />30-130 <br />30 <br />%SS4: <br />N/A <br />5 <br />N/A <br />N/A <br />N/A <br />76 <br />76 <br />0 <br />N/A <br />N/A <br />30-130 <br />30 <br />%SS5: <br />N/A <br />5 <br />N/A <br />N/A <br />N/A <br />118 <br />111 <br />6.29 <br />N/A <br />N/A <br />30- 130 <br />30 <br />%SS6: <br />N/A <br />5 <br />N/A <br />N/A <br />N/A <br />90 <br />90 <br />0 <br />N/A <br />I N/A <br />1 30-130 <br />30 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />BATCH 33632 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br />0801699-001A 01/29/08 10:05 AM 02/05/08 02/07/08 11:27 PM <br />= Matrix Spike; MSD = Matrix Spike Duplicate: LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; <br />Recovery = 100' (MS -Sample) / (Amount Spiked); RPD = 100' (MS - MSD) I ((MS . MSD) 121. <br />3 / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample Is inhomogenous AND contains <br />= not enough sample to perform matrix spike and matrix spike duplicate. <br />INK=anaivie concenurimon in samPie exceaus sDisa <br />DH8-BLAPCertifieationN°-1644 --- A QA/QC,0ffirPr. <br />
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