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534 Willow Pass Road,Pittsburg,CA 94565-1701 Web:wwwmccampbell.com E-mail:nuin@mecampbell.com "When Oaaliw Counts" Telephone:877-252-9262 Fax:925-252-9269 MCCampbell Analytical, IIIc. NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 Terminal Waste Date Received: 05/05/08 1100 Willow Pass Road Client Contact: Dan Thomas Date Extracted: 05/13/08-05/14/08 Pittsburg,CA 94565 Client P.O.: #4501224877 Date Analyzed 05/14/08 Semi-Volatile Organics by GC/MS(Basic Target List)[TCLP Extractlonl* Extraction Method: SW1311/SW3510C Analytical Method: SW827GD Work Order: 0805110 Lab ID 0805110-001A Client ID 29080312-01 Matrix Soil Reporting Reposing Compound Concentration* DF Limit Compound Concentration* DF Limit Acenaphthene ND<0.020 2.0 0.01 Acenaphthylene ND<0.020 2.0 0.01 Anthracene ND<0.020 2.0 0.01 Benzidine ND<O.10 2.0 0.05 Benzoic Acid ND<0.10 2.0 0.05 Benzo(a)anthracene ND<0.020 2.0 0.01 Benzo b fluoranthene ND<0.020 2.0 0.01 Benzo k fluoranthene ND<0.020 2.0 0.01 Benzo h i e lene ND<0.020 2.0 0.01 Benzo(a)pyrene ND<0.020 2.0 0.01 Benzyl Alcohol ND<0.040 2.0 0.02 1 I-Bi hen 1 ND<0.020 2.0 0.01 Bis 2-chloroethoz Methane ND<0.020 2.0 0.01 Bis 2-chloroeth I Ether ND<0.020 2.0 0.01 Bis 2-chloroiso ro 1 Ether ND<0.020 2.0 0.01 Bis 2-eth [hex I Phthalate ND<0.040 2.0 0.02 4-Bromo hen 1 Phenyl Ether ND<0.020 2.0 0.01 Bu Ibenz I Phthalate ND<0.020 2.0 O.OI 4-Chloroaniline ND<0.040 2.0 0.02 4-Chloro-3-meth 1 henol ND<0.020 2.0 0.01 2-Chlorona hthalene ND<0.020 2.0 0.01 2-Chlorophenol ND<0.020 2.0 0.01 4-Chloro hen I Phenyl Ether ND<0.020 2.0 0.01 Ch Bene ND<0.020 2.0 0.01 Dibenzo a,h anthracene ND<0.020 2.0 0.01 Dibenzofuran ND<0.020 2.0 0.01 Di-n-but I Phthalate ND<0.020 2.0 0.01 1,2-Dichlorobenzene ND<0.020 2.0 0.01 13-Dichlorobenzene ND<0.020 2.0 O.OI 14-Dichlorobenzene ND<0.020 2.0 0.01 3 3-Dichlorobenzidine ND<0.040 2.0 0.02 2 4-Dichloro henol ND<0.020 2.0 0.01 Diethyl Phthalate ND<0.020 2.0 0.01 2,4-Dimethylphenol ND<0.020 2.0 0.01 Dimethyl Phthalate ND<0.020 2.0 0.01 4 6-Dinitro-2-meth I henol ND<0.10 2.0 0.05 2 4-Dinitro henol ND<0.10 2.0 0.05 2 4-Dinitrotoluene ND<0.020 2.0 0.01 2 6-Dinitrotoluene ND<0.020 2.0 0.01 Di-n-oct 1 Phthalate ND<0.020 2.0 0.01 1 2-Di hen Ih drazine ND<0.020 2.0 0.01 Fluoranthene ND<0.020 2.0 0.01 Fluorene ND< .020 2. 001 Hex hl ro n ND<0.020 2.0 0.01 Hexachlorobutadiene ND<0.020 2.0 0.01 Hexachloroc clo entadiene ND<0.02 2.0 0.01 H xachloroethane ND<0.020 2.0 0.01 Indeno(1,2,3-cd) rene ND<0.020 2.0 0.01 Iso h r ne D< . 2 2- th In hth I ND<0.020 2.0 0,01 2-Meth I henol(o-Cresol) ND<0.020 2.0 0.01 3&/or 4-Meth I henol(m.n-Cres ND<0.020 2.0 0.01 Naphthalene ND<0.020 2. 1 -Ni r aniline ND<0.10 2.0 0.05 3-Nitroaniline ND<O.10 2.0 0.05 4-Nitroaniline ND<0.10 2.0 0.05 2- itro henol < .10 2.0 0.054- i r henol ND<0.020 2.0 0.01 Nitrobenzene ND<0.10 2. N-Nitr i h n lamin ND<0.020 2.0 0.01 N-Nitrosodi-n- ro lamine ND<0.020 2.0 0.01 Pentachlorophenol ND<0.10 2.0 0.05 Phenanthrene ND< . 2 .01 Phenol ND<0.020 2.0 0.01 Pyrene ND<0.020 2.0 0.01 1 2 4-Tri hlor nzene ND<0.020 2.0 0.01 < ND<1020 2.0 Surrogate Recoveries(%) %SSI, 83 %SS2: 76 %SS3 75 4: 78 Comments: I *water samples in pg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,product/oil/non-aqueous liquid samples and all TCLP& SPLP extracts are reported in mg/L. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. #)surrogate diluted out orange;&)low or no surrogate due to matrix interference. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to hi h organic content/matrix interference. DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager