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1534 McCampbell Analytical, Inc. www.me1ow PassRoad,Pittsburg,:noun 94565-1701 !�[,_.� Web: &rtuil:rmivQ°mecampbea.wm a� 'When O IiNCourts" Telephone:877-252-9262 Fax:925-252-9269 NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 Terminal Waste Date Received: 05/05/08 1100 Willow Pass Road Client Contact: Dan Thomas Date Extracted: 05/13/08-05/14/08 Pittsburg,CA 94565 Client P.O.: #4501224877 Date Analyzed 05/14/08 Semi-Volatile Organics by GC/MS(Basic Target List)ITCLP Extraction]* Extraction Method: SW1311/SW3510C Analytical Method: SW8270D Work Order. 0805110 Lab ID 0805110-002A Client ID 29080312-02 Matrix Soil Compound Concentration " DF Repmang Cd Concentration• DF Re Lie i Compound Limit P Limit Acena hthene ND<0.020 2.0 0.01 Acena hth lene ND<0.020 2.0 0.01 Anthracene ND<0.020 2.0 0.01 Benzidine ND<O.10 2.0 0.05 Benzoic Acid ND<0.10 2.0 0.05 Benzo(a)anthracene ND<0.020 2.0 0.01 Benzo b Buoranthene ND<0.020 2.0 0.01 Benzo k tluoranthene ND<0.020 2.0 0.01 Benzo h i e lene ND<0.020 2.0 0.01 Benzo(a)pyrene ND<0.020 2.0 0.01 Benz (Alcohol ND<0.040 2.0 0.02 1 1-Biphenyl ND<0.020 2.0 0.01 Bis 2-chloroethoz Methane ND<0.020 2.0 0.01 Bis 2-chloroeth I Ether ND<0.020 2.0 0.01 Bis 2<hloroiso ro 1 Ether ND<0.020 2.0 0.01 Bis 2-eth (hex 1 Phthalate ND<0.040 2.0 0.02 4-Bromo hen I Phenyl Ether ND<0.020 2.0 0.01 But Ibenz 1 Phthalate ND<0.020 2.0 0.01 4-Chloroaniline ND<0.040 2.0 0.02 4-Chloro-3-meth 1 henol ND<0.020 2.0 0.01 2-Chlorona hthalene ND<0.020 2.0 0.01 2-Chlorophenol ND<0.020 2.0 0.01 4-Chloro hen 1 Phenyl Ether ND<0.020 2.0 0.01 Chrysenc ND<0.020 2.0 0.01 Dibenzo a h anthracene ND<0.020 2.0 0.01 Dibenzofuran ND<0.020 2.0 0.01 Di-n-but I Phthalate ND<0.020 2.0 0.01 12-Dichlorobenzene ND<0.020 2.0 0.01 13-Dichlorobenzene ND<0.020 2.0 0.01 14-Dichlorobenzene ND<0.020 2.0 0.01 7 3-Dichlorobenzidine ND<0.040 2.0 0.02 2 4-Dichlorophenol ND<0.020 2.0 0.01 Diethyl Phthalate ND<0.020 2.0 0.01 2,4-Dimethylphenol ND<0.020 2.0 0.01 Dimeth 1 Phthalate ND<0.020 2.0 0.01 4 6-Dinitro-2-meth I henol ND<0.10 2.0 0.05 2 4-Dinitro henol ND<0.10 2.0 0.05 2 4-Dinitrotoluene ND<0.020 2.0 0.01 2 6-Dinitrotoluene ND<0.020 2.0 0.01 Di-n-octyl Phthalate ND<0.020 2.0 0.01 1 2-Di hen lh drazine ND<0.020 2.0 0.01 1 Fluoranthene ND<0.020 2.0 0.01 Fluor ne ND<0.020 2.0 0.01 Hex ch r ND<0.020 2.0 0.01 Hexachlorobutadiene D<0.020 2.0 0.01 Hexachloroc clo entadiene ND<0.020 2.0 0.01 Hexachl roethan ND<0.020 2.0 0.01 Indeno(1,2.3-cd)pyrene ND<0.020 2.0 0.01 lsophoTone ND<OwO2O 2.0 0.01 2-M ethyl nhth alents ND<0.0202.0 0.01 2-Meth I henol(o-Cresol) ND<0.020 2.0 0.01 3&/or 4-Meth I henol(m,P-Cres ND<0.020 2.0 0.01 Naphthalene ND<0.020 2.0 0.01 2-Nitroaniline ND<0.10 2.0 0.05 3-Nitroaniline D<0.10 2.0 0.05 4-Nitroaniline ND<0.10 2.0 0.05 2-Nitro hen I ND<O.10 .0 4-Niro enol ND<0.020 2.0 0.01 Nitrobenzene ND<0.10 2.0 0 UL N-Nitroso i h famine ND<0.020 2.0 0.01 N-Nitrosodi-n- ro lamine ND<0.020 2.0 70.01 Pentachlorophenol ND<0.10 2.0 0.05 Phenan hr n D<0.020 2.0 1 0.01 1 Phenol < . 20 2.0 0.01 P r n ND<0.020 2.0 1 OwOl 1 4-Trichl ro n ND< < 1 < Surrogate Recoveries(%) 82 2: 66 2 1 ° S4S4 75 Comments: i *water samples in pg/L,soil/sludge/solid samples in mg/kg,wipe samples inµp/wipe,product/oil/non-aqueous liquid samples and all TCLP& SPLP extracts are reported in mg/L. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. #)surrogate diluted out of range;&)low or no surrogate due to matrix interference. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-I vol.%sediment;j)sample diluted due to hi h organic content/matrix interference. DHS ELAP Certification No 1644 A2- Angela Rydelius,Lab Manager