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McCampbell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 (��.i Web:www.mccampbell.com E-mail:main@mccampbell.com "When Oualits Counts' I Telephone:877-252-9262 Pax:925-252-9269 NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 Terminal Waste Date Received: 05/05/08 1100 Willow Pass Road Client Contact: Dan Thomas Date Extracted: 05/05/08-05/06/08 Pittsburg,CA 94565 Client P.O.: #4501224877 Date Analyzed 05/10/08 Volatile Organics by GUMS(Basic Target List)[ZHETCLP Extraction[* Extraction Method: SW1311(ZHETCLP)/SW5030B Analytical Method: SW8260B Wark Order. 0805110 Lab ID 0805110-002A Client ID 29080312-02 Matrix Soil Comtiound ConcentrationDF xepomng ompoun Cd Concentra �tion DF aepnnfng � L' Limit Acetone ND 1.0 0.2 t r-Am 1 methyl e her TAME ND 1.0 0.0005 Benzene ND 1.0 0.0005 Bromobenzene ND 1.0 0.0005 Bromochloromethane ND 1.0 0.0005 BromodiChIOTometharic ND 1.0 0.0005 Br m form ND 1.0 U005 Bromomethane ND 1.0 0.0005 2-B t o n EK D 1.0 0.5 t- ut I alcohol TBA NQ Lo 0.05 ii-Butyl benzene ND 1.0 0,0005 ee-But I benzene ND 1.0 0,0005 tert-But 1 benzene ND 1.0 0.0005 Carbon Disulfide ND 1.0 0.0005 Carbon Tetrachloride ND 1.0 0,0005 Chlorobenzene NQ 1.0 00005 Chloroethane ND 1.0 0,0005 Chloroform ND 1.0 0.0005 ChloromethaneND 1.0 InE00512-Chlorotoluene ND 1 1.0 0.0005 4-Chlorotoluene ND 1.0 0.00051 Dibromachloromethane ND 1.0 0.0005 12-Dibromo-3-chloro ro ane ND 1.0 0.0005 12-Dibromoethane EDB ND 1.0 0.0005 Di ro h ND I. 0 0005 12-Di hlor n n D 1. 0.0005 13-Dichlorobenzene ND 1.0 0.0005 1.4-Dichlorobenzene ND 1.0 0.0005 i h ro ifl oromethan ND 1.0 00005 I I-Dichloroeth n ND I. 0. 005 1 2-Dichloro than (1,2-DCA) ND 1.0 0.0005 I -Di hl r then D I. 0 0005 cis-I 2-Dichlor thene ND 1.0 0.0005 trans-1 2-Dichloroethene ND I.0 0.0005 1 2-Dichloro ro ane ND 1. 0.0005 I -Dichloro r ane 1. 0000 5 22-Dichloro ro ane ND 1.0 0.0005 1 1-Dichloro ro ene ND 1.0 0.0005 cis-1 - i h r ro ene ND 1. 0,0005 trans-I 3-Diehl r ro ne N 0 0005 Dii o ro I ether DIPE ND 1.0 Or0005 EthylbenzeneND 1 0.0005 Ethyl t rt- t l ether B ND 1. 0.0005 Freon 113 N D .0 0.01 H c or b t di n ND 0,0005 Flx Ire n N 0 0005 2-Hexanone ND 1.0 0.02 Is ro (benzene ND LO 0.0005 4-Isopropyl of N 1. 0.0005 Meth I-t-bu ether MTBE N 1. 0.0005 Methylene chloride ND 1.0 0.005 4-Meth I-2- entanone MIBK ND 1.0 0.005 N ht 0.0015 1. 0005 -Pr I enzen D 1. 0.0005 Styrene D I. 0.0005 1 1 1 2- ra hl r h ne ND I. 0 0005 1122-Tetrachloroethane ND 1.0 0.0005 Tetrachloroethene ND 1.0 0.005 Toluene ND 10 0.005 1 i hl r nzene D 1 0 100005 1 2 4-Trichlorobenzene ND 1.0 0.0005 1 1 I-Trichloroethane ND 1.0 0.0005 1 1.2-Trichloroethane D 1.0 0.0005 Trichl meth 0 0,005 Trichlorofluoromethane ND LO 0.0005 1 2 3-Trichlorc tartaric ND I.0 0.0005 4-Trim th I benzene 0.0043 0 005 1 3 5-Trime nz 0,0029 I.0 0 0005 Surrogate Recoveries %SSI: 102 %SS2: 97 Comments: e water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts are reported in mg/L,wipe samples in pg/wipe. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. #surrogate diluted out of range or surrogate coelutes with another peak;&)low surrogate due to matrix interference. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) reporting limit raised due to insufficient sample amount;n results are reported on a dry weight basis; )see attached narrative. DHS ELAP Certification No 1644 J2- Angela Rydelius,Lab Manager