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McCamobell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 Web:www.mccampbell.com E-mail:mainQmuampbell.com 4;2 "When Oualty Counts' I Telephone:877-252-9262 Fax:925-252-9269 NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 Terminal Waste Date Received: 05/05/08 1100 Willow Pass Road Client Contact: Dan Thomas Date Extracted: 05/05/08-05/06/08 Pittsburg,CA 94565 Client P.O.: #4501224877 Date Analyzed 05/10/08 Volatile Organics by GUMS(Basic Target List)[ZHETCLP Extraction]* Extraction Method: SW1311(ZHETCLP)/SW5030B Analytical Method: SW8260B Work Order. 0805110 Lab ID 0805110-001A Client ID 29080312-01 Matrix Soil Comoound Concentration*I DF RCLomntg I Comoound ConcentrationDF I RqLwi.;;B Acetone ND I. 0 tort-Am 1 ethyl r(TAME) ND 1.0 0.0005 Benzene ND 1.0 0.0005 Bromobenzene ND 1.0 0.0005 Br hl romelhane ND 1.0 0,0005 Br modichlor m t an D 1. 0.0005 Bro f r ND 1.0 0.0005 Hr m m hart 1.0 0,000 2-Butan ne MEK L0 0.5 t-B [ I I TBA ND 0 n-B t l benzeneI. 00 sec-Butyl N 0,000 tert-But I benzene ND LO 0,0005 Carbon Disulfide ND 1.0 0.0005 Carbon Tetr 1.0 0.0005 I r n n N 1. 0,000 Chloroethane ND 1.0 0 0005 Chloroform ND 1.0 0.0005 Chloromethane ND 1.0 0,0005 2-Chlorotoluene NQ 1.0 10.00051 4-Chlorotoluene ND 1.0 0.0005 Dibromochloromethane ND 1.0 0,000 12-Dibromo- -chloro ro ane ND 1.0 10.0005 1 2-Dibromoethane EDA ND 1.0 0,000 Dibromonrotthane ND 1.0 10 0005 1.2-Dichlorobenzene D 1.0 0.0005 13-Dichlorobenzene ND 1.0 10,0005 1.4-Dichlorobenzene ND 1.0 0.0005 DichlQuidifluoromethane ND 1.0 0.0005 1.1-Dichloroethane N Q 1.0 0.0005 1 2-Diehl r h ne(1.2-DCA) ND 1.0 0,0005 -D' I r hene ND 1.0 0.0005 cis-1 2-Dichloroethene ND 1.0 0,0005 bans-I 2-Dichloroethene ND 1.0 0.0005 1.2-Dichloropropanc ND 1.0 0,0005 1.3- ihl ro r an ND 1.0 0.0005 7 2-Dichloro ro ane ND 1.0 0.0005 1 I-Di hloro ro ene ND 1.0 0,000 cis-1,3-Diclr0oroproramc ND 1.0 0,0005 a -13-Dichloroortmene ND 1.0 10 00051 Dii o ro I ether DIP ND 1.0 0.00051 Eth I enzene 0.00051 1.0 0,000 Ethyl tort-bu ETBE D LO 0 0051 Freon 113 ND 1.0 0,01 Hcxachlorobutadiene NQ 1.0 0,0005 H xachl r et an ND 1.0 0,0005 2-Hexanone ND 1.0 0.02 ISOPTanylbenzene ND 1.0 0.0005 4-Isopropyl toluene ND 1.0 U005 M h l-t- u t NIB ND 1.0 0.0005 Methylene chloride ND 1.0 0.005 4-Meth 1-2- ent n ne MIBK ND Lo 0.005 Naphthalene 0.002 1.0 0.0005 P-Propyl benzene ND 1.0 0.000 Styrene ND 1.0 0.0005 1 1 2-T trachlor ethane NQ Lo 0.000 t.1,2,2-Tetrachloroethane ND 1.0 0.0005 Tetrachloroethene ND 1 1.0 1 0.005 Toluene ND 1.0 005 1.2.3-Trichlortiberizene ND 1.0 0.0005 1 2 4-Trichlor benzene ND 1.0 0.0005 1.1.1-Trichloroethane ND 1.0 0.0005 I.1.2-Trichloroethane ND0 0 005 Tri hlor h n ND 1.0 0.005 Trichloroftuor methane ND L0 0.0005 1 2 3-Trichloro ro ane ND .2O 1 2 4-Trimeth (benzen 0.011 10 10,00051 1 3 5-Trime I n 0 005 0 0 0005 Surrogate Recoveries Sl: TI 102 %SS2: 97 0 Comments -water and vapor samples are reported in pg(L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts are reported in mg/L,wipe samples in pg/wipe. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. k surrogate diluted out of range or surrogate coelutes with another peak;&)low surrogate due to matrix interference. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; see attached narrative. DHS ELAP Certification No 1644 J2- Angela Rydelius,Lab Manager