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' Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2112012 Date: 12/04/2002 Page: 1 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-1 Lab Samp ID: 32205-001 <br /> Descr/L.ocation: MW-1 Recd Date: 11/2212002 <br /> Sample Date: 11/19/2002 Prep Date: 11/27/2002 <br /> ' Sample Time: 1205 Analysis Date: 11/27/2002 <br /> Matrix: Water QC Batch: WMS21821 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tart-butyl ether(MTBE) 0.3 1. PQL 1.7 UG/L 1 <br /> ' Ethyl Cert-butyl ether(ETRE) 0.5 5. PQL ND UG/L 1 <br /> ter#-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10. PQL ND UG/L 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UG/L 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMSA 100.3% 1 <br /> Toluene-d8 77-150 SMEA 103.2% 1 <br /> Dlbromofluoromethane 57156 SMEAAZ 0% ! 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> 1 <br /> 1 <br /> Approved by: th Date: � 'V—'-- <br />