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1 I <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> ' Lab Report No.: H2112012 Date: 12/04/2002 Page: 2 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-101 Lab Samp ID: 32205-002 <br /> Descr/Location: MW-101 Recd Date: 11/22/2002 <br /> Sample Date: 11/19/2002 Prep Date: 11/27/2002 <br /> ' Sample Time: 1227 Analysis Date: 11/27/2002 <br /> Matrix: Water QC Batch: WMS21821 <br /> Basis: Not Filtered Notes: <br /> 1 Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL ND UGIL 1 <br /> ' Ethyl tert-butyl ether(ETBE) 0.5 S. PQL ND UGIL 1 <br /> tent-Amyl methyl ether(TAME) 0.3 5. PQL ND UG1L 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 1 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMSA 96.1% 1 <br /> Toluene-d8 77-150 SMEA 104.5% 1 <br /> Zromofluoromethane 57-156 SMEAAZ 0% i 1 <br /> : Surr. recovery outside of acceptance limits due to matrix interf. <br /> 1 <br /> 1 <br /> Approved by: - -- Date: y1aZ4L'7 <br /> 1 <br />