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Entech Analytical Lags, Inc., Santa Clara, CA <br /> Lab Report No.: H2112012 Date: 12/04/2002 Page: 3 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2 Lab Samp ID: 32205-003 <br /> Deser/Location: MW-2 Ree'd Date: 1112212002 <br /> Sample Date: 11/19/2002 Prep Date: 11/27/2002 <br /> ' Sample Time: 1301 Analysis Date. 11/27/2002 <br /> Matrix: Water QC Batch: WMS21821 <br /> Basis: Not Filtered Notes: <br /> tAnalyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 1. PQL ND UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> DI-isopropyl ether(DIPE) 0.5 5. PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 4.6 10, PQL ND UGIL. 1 <br /> 1,2-Dichloroethene 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMSA 97.0% 1 _ <br /> Toluene-d8 77-150 SMEA 105.2% ; <br /> Dib romofluoromethane 57-156 SMEAAZ 0.2% 1 T. <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> 1 <br /> I <br /> 1 <br /> Approved by: LAP2 Date: <br />