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Entech Analytical Labs, Inc., Santa Clara, CA <br /> bReport No.: H2092702 Date: 10110/2002 Page:4 <br /> ' Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GCIMS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth. SW5030B <br /> ' Field ID: MW-4 . Lab Samp ID: 31458-003 <br /> Descr/L.ocation: MW-4 Recd Date: 10/08/2002 <br /> Sample Date: 09/26/2002 Prep Date: 10/03/2002 <br /> ' Sample Time: 1010 Analysis Date: 10/0312002 <br /> Matrix: Water QC Batch: WMS11733 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 5, PQL 14. UGIL 1 <br /> Ethyl tert-butyl ether(ETRE) 0.5 5. PQL ND UGIL 1 <br /> tent-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 11. 20. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 03 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65.135 SMEA 103.7% 1 <br /> Toluene-d8 77-150 SMEA 111.7° 1 <br /> Dibromofluoromethane 57-156 SMEA 116.2% 1 <br /> 1 <br /> 1 <br /> t <br /> lj I <br /> Approvea Dy:_ '�' �� uate: <br />