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' Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2092702 Date: 10/10/2002 Page: 5 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-5 Lab Samp ID: 31458-002 <br /> DescrlLocation: MW-5 Recd Date: 10/08/2002 <br /> Sample Date: 09/26/2002 Prep Date: 10/03/2002 <br /> ' Sample Time: 0937 Analysis Date: 10/03/2002 <br /> Matrix: Water QC Batch: WMS11733 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc DiI <br /> Methyl-tent-butyl ether(MTBE) 0.3 5. PQL 5Ek UG/L 1 <br /> ' Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> DI-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 11. 20. PQL ND UG/L 1 <br /> 1 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UG/L 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Brom ofluoro benzene 65-135 SMEA 911.0° <br /> Toluene-d8 77-150 SMEA 112.7° 1 <br /> Dibromofluoromethane 57-156 SMEA 116.9% 1 <br /> Approves qy: i�' ' Uate: l I�! L <br />