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1 <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2O82605 Date: 09/05/2002 a Page: 2 <br /> ' Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 428409E Method: 8260FA <br /> Prep Meth: SW5030B <br /> tField ID: MW-7 Lab Samp ID: 31020-002 <br /> Descr/Location: MW-7 Rec'd Date: 08/26/2002 <br /> ' Sample Date: 08/22/2002 Prep Date: 08/2812002 <br /> Sample Time: 1122 Analysis Date: 08/28/2002 <br /> Matrix: Water QC Batch: WMS21686 <br /> ' Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 5. PQL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UG/L 1 <br /> tert-Butyl alcohol (CBA) 11. 20. PQL ND UGIL 1 <br /> 1,2-Dichioroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-131bromoethane 1 0.5 5. PQL ND UG/L 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 95.3% 1 <br /> Toluene-d8 77-150 SMEA 98.7% 1 <br /> Dibromofluoromethane 57-156 SMEA 98.4% 1 <br /> Approved by: ) fu Date: a q- L <br />