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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2082605 Date: 09/05/2002 Page: 3 <br /> ' Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 429409E Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-8 Lab Samp ID: 31020-003 <br /> Descr/Location: MW-8 Recd Date: 08/2612002 <br /> ' Sample Date: 08/22/2002 Prep Date: 08128/2002 <br /> Sample Time: 1203 Analysis Date: 08/28/2002 <br /> Matrix: Water QC Batch: WMS21686 <br /> ' Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) d.3 5. PQL 17 UG/L 1 <br /> Ethyl tent-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UG/L 1 <br /> tent-Butyl alcohol (TBA) 11. 20. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 12-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65135 SMEA 96.0% 1 <br /> Toluene-d8 77-150 SMEA 99.7% 1 <br /> Dibromofluoromethane 57-156 SMEA 92.0% 1 <br /> 1 <br /> Approved by: / LSI^1 '�� Date: <br />