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ANALYTICAL RESULTS I/GTEL Client ID CES06CE506 Total Petroleum Hydrocarbons By GC login Number W7070538 Project ID (number) 97735 Method GC Project ID (name) CANONIE/DIESEL PERFORMANCE/MODESTO/CA Matrix Solids NEI/GTEL Sample Number W7070538 05 W7070538-06 _ W7070538-07 W7070538 08 Client ID DP-SB3 30 0 DP SB3-45 0 DP-SB4-15 0 DP-SB4-30 0 Date Sampled 07/23/97 07/23/97 07/23/97 07/23/97 Date Prepared 08/02/97 08/02/97 08/02/97 08/02/97 Date Analyzed 08/07/97 08/07/97 08/07/97 08/07/97 Dilution Factor 1 00 1 00 1 00 1 00 Reporting Analyte Limit Units Concentration Wet Weight TPH as Kerosene 10 mg/kg < 10 < 10 < 10 < 10 TPR as Olesel 10 mg/kg < 10 < 10 < 10 < 10 TPH as Lubricating Oil 10 mg/kg < 10 < 10 < 10 < 10 Percent Solids -- 75 9 81 6 75 6 92 5 Motes Dilution Factor Dilution factor indicates the adjustments made for sample dilution GC Extraction by EPA Method 3550 (sonication) ASTM Method 03328(modified) is used for qualitative identification of fuel patterns The method has been modified to include quantitation by applying calibration and quality assurance guidelines outlined to "Test Methods for Evaluating Solid Waste Physical/Chemical Methods SW 846 Third Edition including promulgated Update 1 This method 3s equivalent to the California LUFT manual OHS method or diesel fuel Due to the qualitative similarities between Kerosene and Diesel Fuel the material present was quantified only as the product which it most resembled chromatographically The reporting limit for the other analyte was elevated accordingly Lubricating oil can not be qualitatively identified by type of oil because of chromatographic likeness of different oil types Due to non volatility of certain oils much of the oil present may not be quantified by this method Quantitation obtained for lubricating oil by this method should therefore be treated as an estimate This method quantifies lubricating oil against 10-W-30 standards I/GTEL Wichita KS X17070538 Page 2