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-F it '■ ANALYTICAL RESULTS II/GTEL Client ID CE506CE506 Total Petroleum Hydrocarbons By GC gin Number W7070538 Project ID (number) 97735 Method GC Project ID (name) CANONIE/DIESEL PERFORMANCE/MODESTO/CA Matrix Solids NEI/GTEL Sample Number W7070538 09 W7070538 10 Client ID DP-S65 15 0 DP S85 30 0 - Date Sampled 07/23/97 07/23/97 Date Prepared 08/02/97 08/02/97 Date Analyzed 08/07/97 08/07/97 -- Dilution Factor 1 00 1 00 - Reporting Analyte Limit Units Concentration Wet Wei ht TPH as Kerosene 10 mg/kg < 10 < 10 -- -- TPH as Diesel 10 mg/kg < 10 < 10 -- -- TPR as Lubricating Oil 10 mg/kg < 10, < 10 -- -- Percent Solids -- % 78 1 75 4 -- -- Notes Dilution Factor Dilution factor indicates the adjustments made for sample dilution GC Extraction by EPA Method 3550 (sonication) ASTM Method 03328(modified) is used for qualitative identification of fuel patterns The method has been modified to include quantitation by applying calibration and quality assurance guidelines outlined in "Test Methods for Evaluating Solid Waste Physical/Chemical Methods SW-846 Third Edition including promulgated Update 1 This method is equivalent to the California LUFT manual DHS method Omor diesel fuel Due to the qualitative similarities between Kerosene and Diesel Fuel the material present was quantified only as the product which it ost resembled chromatographically The reporting limit for the other analyte was elevated accordingly Lubricating oil can not be qualitatively identified by type of oil because of chromatographic likeness of different oil types Due to non-volatility of certain oils much of the oil present may not be quantified by this method Quantitation obtained for lubricating oil by this method should therefore be treated as an estimate This method quantifies lubricating oil against 10-W-30 standards I/GTEL Wichita KS 7070538 Page 3