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Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7714-1 <br /> Client Sample ID: NW1-3' <br /> Lab Sample ID: 720-7714-1 Date Sampled: 02/12/2007 1400 <br /> Client Matrix: Solid Date Received: 02/12/2007 1720 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch:720-18250 Instrument ID: Varian 3900A <br /> Preparation: 5030B Prep Batch: 720-18249 Lab File ID: c:\saturnws\data\200702\02 <br /> Dilution: 200 Initial Weight/Volume: 5.03 g <br /> Date Analyzed: 02/14/2007 0152 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/13/2007 0945 <br /> Analyte DryWt Corrected: N Result(mg/Kg) r Qualifier RL - <br /> Benzene ND 0.99 <br /> Ethylbenzene ND 0.99 <br /> Toluene ND 0.99 <br /> MTBE ND 0.99 <br /> Xylenes,Total ND 2.0 <br /> Gasoline Range Organics(GRO)-C5-C12 300 50 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8(Surr) 89 50-130 <br /> 1,2-Dichloroethane-d4(Surr) 99 6.0- 140 <br /> r <br /> a <br /> 1 <br /> 5 <br /> I <br /> 1 <br /> l <br /> I <br /> Page 7 of 21 <br /> STL San Francisco <br />